Silane, bicyclo[4.4.1]undeca-1,3,5,7,9-pentaen-2-yltrimethyl-

Base Information

• Chemical Name: Silane, bicyclo[4.4.1]undeca-1,3,5,7,9-pentaen-2-yltrimethyl-
• CAS No.: 58081-06-4
• Molecular Formula: C14H18Si
• DSSTox Substance ID: DTXSID801180665
• Nikkaji Number: J1.974.964I

Synonyms:DTXSID801180665;Silane, bicyclo[4.4.1]undeca-1,3,5,7,9-pentaen-2-yltrimethyl-;58081-06-4

Chemical Property of Silane, bicyclo[4.4.1]undeca-1,3,5,7,9-pentaen-2-yltrimethyl-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 214.117777109
• Heavy Atom Count: 15
• Complexity: 204

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C[Si](C)(C)C1=CC=CC2=CC=CC=C1C2

Technology Process of Silane, bicyclo[4.4.1]undeca-1,3,5,7,9-pentaen-2-yltrimethyl-

There total 1 articles about Silane, bicyclo[4.4.1]undeca-1,3,5,7,9-pentaen-2-yltrimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

chloro-trimethyl-silane (75-77-4) + 2-bromo-1,6-methano[10]annulene (15825-92-0,107134-29-2,107134-35-0) → 2-trimethylsilyl-1,6-methano<10>annulene (58081-06-4) + 1,6-methano[10]annulene (2443-46-1)

Guidance literature:

With n-butyllithium; In diethyl ether; hexane; at -50 - -10 ℃;

DOI:10.1016/0022-328X(86)80191-7

Reference yield:

2-trimethylsilyl-1,6-methano<10>annulene (58081-06-4) → 1,6-methano[10]annulene (2443-46-1)

Guidance literature:

With perchloric acid; In methanol; at 50 ℃; Rate constant; effect of acid concentration;

DOI:10.1039/P29880000697

upstream raw materials:

chloro-trimethyl-silane

2-bromo-1,6-methano[10]annulene

Downstream raw materials:

1,6-methano[10]annulene

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