Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 5-[(4-methoxyphenyl)methyl] 3-methyl ester, (1S,2R,3S,4R,5S,6R)-

Base Information

Chemical Name:Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 5-[(4-methoxyphenyl)methyl] 3-methyl ester, (1S,2R,3S,4R,5S,6R)-
CAS No.:581100-38-1
Molecular Formula:C25H35NO9Si
Molecular Weight:521.64
Hs Code.:

Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid,
6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-,
5-[(4-methoxyphenyl)methyl] 3-methyl ester, (1S,2R,3S,4R,5S,6R)-

Synonyms:

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Chemical Property of Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 5-[(4-methoxyphenyl)methyl] 3-methyl ester, (1S,2R,3S,4R,5S,6R)-

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Technology Process of Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 5-[(4-methoxyphenyl)methyl] 3-methyl ester, (1S,2R,3S,4R,5S,6R)-

There total 2 articles about Bicyclo[2.2.1]heptane-2,3,5-tricarboxylic acid, 6-[[[2-(trimethylsilyl)ethoxy]carbonyl]amino]-, 5-[(4-methoxyphenyl)methyl] 3-methyl ester, (1S,2R,3S,4R,5S,6R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 581100-37-0
bicyclo[2.2.1]heptane-2-endo-(4-methoxy)benzyl-3-endo-(trimethylsilylethoxycarbonyl)amino-5-exo-6-exo-dicarboxylic anhydride

: 581100-38-1
bicyclo[2.2.1]heptane-2-endo-(4-methoxy)benzyl-3-endo-(trimethylsilylethoxycarbonyl)amino-5-exo-carboxy-6-exo-methyl dicarboxylate

Guidance literature:: bicyclo[2.2.1]heptane-2-endo-(4-methoxy)benzyl-3-endo-(trimethylsilylethoxycarbonyl)amino-5-exo-6-exo-dicarboxylic anhydride; With quinine; In tetrachloromethane; toluene; at -65 ℃; for 1h;

methanol; In tetrachloromethane; toluene; at -65 ℃; for 96h;

Reference yield:

: 581100-37-0
bicyclo[2.2.1]heptane-2-endo-(4-methoxy)benzyl-3-endo-(trimethylsilylethoxycarbonyl)amino-5-exo-6-exo-dicarboxylic anhydride

: 581100-38-1
bicyclo[2.2.1]heptane-2-endo-(4-methoxy)benzyl-3-endo-(trimethylsilylethoxycarbonyl)amino-5-exo-carboxy-6-exo-methyl dicarboxylate

Guidance literature:: With Quinine; In methanol; tetrachloromethane; toluene;

Reference yield:

: 581100-38-1
bicyclo[2.2.1]heptane-2-endo-(4-methoxy)benzyl-3-endo-(trimethylsilylethoxycarbonyl)amino-5-exo-carboxy-6-exo-methyl dicarboxylate

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 581100-39-2
bicyclo[2.2.1]heptane-2-endo-(4-methoxy)benzyl-3-endo-(trimethylsilylethoxycarbonyl)amino-5-exo-(trimethylsilylethoxycarbonyl)amino-6-exo-methyl dicarboxylate

Guidance literature:: bicyclo[2.2.1]heptane-2-endo-(4-methoxy)benzyl-3-endo-(trimethylsilylethoxycarbonyl)amino-5-exo-carboxy-6-exo-methyl dicarboxylate; With diphenyl phosphoryl azide; triethylamine; In benzene; for 24h; Reflux;

2-(Trimethylsilyl)ethanol; In benzene; for 48h; Reflux;