1,3,2-Oxaazaphospholidine, 2-dimethylamino-3-methyl-

Base Information

• Chemical Name: 1,3,2-Oxaazaphospholidine, 2-dimethylamino-3-methyl-
• CAS No.: 18389-56-5
• Molecular Formula: C5H13N2OP
• Molecular Weight: 148.145
• NSC Number: 171172
• Mol file: 18389-56-5.mol

Synonyms:1,3,2-Oxaazaphospholidine, 2-dimethylamino-3-methyl-;18389-56-5;NSC171172;NSC 171172;NSC-171172;2-(dimethylamino)-3-methyl-1,3,2-oxazaphospholane;Dimethyl-(3-methyl-[1,3,2]oxazaphospholidin-2-yl)-amine

Chemical Property of 1,3,2-Oxaazaphospholidine, 2-dimethylamino-3-methyl-

Chemical Property:

• Vapor Pressure: 2.95mmHg at 25°C
• Boiling Point: 156°Cat760mmHg
• Flash Point: 48.2°C
• Density: g/cm³
• XLogP3: 0.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 148.07655004
• Heavy Atom Count: 9
• Complexity: 99

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1CCOP1N(C)C

Technology Process of 1,3,2-Oxaazaphospholidine, 2-dimethylamino-3-methyl-

There total 2 articles about 1,3,2-Oxaazaphospholidine, 2-dimethylamino-3-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-hydroxyethyl)(methyl)amine (109-83-1) + N,N-dimethylaminodichlorophosphane (683-85-2) → dimethyl-(3-methyl-[1,3,2]oxazaphospholidin-2-yl)-amine (18389-56-5)

Guidance literature:

With triethylamine; In benzene;

Reference yield:

(2-hydroxyethyl)(methyl)amine (109-83-1) + Hexamethylphosphorous triamide (1608-26-0) → dimethyl-(3-methyl-[1,3,2]oxazaphospholidin-2-yl)-amine (18389-56-5)

Guidance literature:

DOI:10.1021/ja00758a034

Reference yield:

dimethylketene (598-26-5) + dimethyl-(3-methyl-[1,3,2]oxazaphospholidin-2-yl)-amine (18389-56-5) → 5-dimethylamino-2,4-diisopropylidene-9-methyl-1,3,6-trioxa-9-aza-5λ5-phospha-spiro[4.4]nonane (37521-12-3)

Guidance literature:

In ethyl acetate;

DOI:10.1021/ja00764a029

upstream raw materials:

(2-hydroxyethyl)(methyl)amine

N,N-dimethylaminodichlorophosphane

Hexamethylphosphorous triamide

Downstream raw materials:

2-methoxy-3-methyl-1,3,2-oxazaphospholidine

5-dimethylamino-2,4-diisopropylidene-9-methyl-1,3,6-trioxa-9-aza-5λ⁵-phospha-spiro[4.4]nonane

5-dimethylamino-9-methyl-2,3-diphenyl-1,4,6-trioxa-9-aza-5λ⁵-phospha-spiro[4.4]non-2-ene

5-methoxy-2,6,9-trimethyl-3-phenyl-1,4-dioxa-6,9-diaza-5λ⁵-phospha-spiro[4.4]non-2-ene