2-bromo-N-(3-methoxyphenyl)benzamide

Base Information

Chemical Name:2-bromo-N-(3-methoxyphenyl)benzamide
CAS No.:58494-94-3
Molecular Formula:C₁₄H₁₂BrNO₂
Molecular Weight:306.159
Hs Code.:
DSSTox Substance ID:DTXSID30355272
Wikidata:Q27186864
ChEMBL ID:CHEMBL1529274

Synonyms:2-bromo-N-(3-methoxyphenyl)benzamide;58494-94-3;2-Bromo-N-(3-methoxy-phenyl)-benzamide;Benzamide, 2-bromo-N-(3-methoxyphenyl)-;MLS001207887;SMR000504856;Cambridge id 5329120;Oprea1_305310;Oprea1_312144;cid_795409;SCHEMBL1499642;CHEMBL1529274;BDBM53043;DTXSID30355272;CHEBI:108187;HMS2825K11;STK031356;AKOS000183079;2-bromanyl-N-(3-methoxyphenyl)benzamide;AB00080981-01;A1-05014;Q27186864

Suppliers and Price of 2-bromo-N-(3-methoxyphenyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-bromo-N-(3-methoxyphenyl)benzamide

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:305.00514
Heavy Atom Count:18
Complexity:285

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1)NC(=O)C2=CC=CC=C2Br

Technology Process of 2-bromo-N-(3-methoxyphenyl)benzamide

There total 3 articles about 2-bromo-N-(3-methoxyphenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 7154-66-7
2-bromobenzoic acid chloride

: 58494-94-3
2-bromo-N-(3-methoxyphenyl)benzamide

Guidance literature:: In dichloromethane; at 21 - 23 ℃; for 12h; Alkaline conditions; Inert atmosphere;
DOI:10.1021/jacs.5b07726

Reference yield:

: 88-65-3
2-bromobenzoic-acid

: 58494-94-3
2-bromo-N-(3-methoxyphenyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / benzene / 0 - 23 °C / Inert atmosphere

2: dichloromethane / 12 h / 21 - 23 °C / Alkaline conditions; Inert atmosphere

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; benzene;
DOI:10.1021/jacs.5b07726