1-Methoxy-3-phenylnaphthalene

Base Information

• Chemical Name: 1-Methoxy-3-phenylnaphthalene
• CAS No.: 59115-41-2
• Molecular Formula: C17H14O
• Molecular Weight: 234.298
• DSSTox Substance ID: DTXSID70566421
• Wikidata: Q82452020
• Mol file: 59115-41-2.mol

Synonyms:1-Methoxy-3-phenylnaphthalene;59115-41-2;DTXSID70566421

Chemical Property of 1-Methoxy-3-phenylnaphthalene

Chemical Property:

• PSA: 9.23000
• LogP: 4.51540
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 234.104465066
• Heavy Atom Count: 18
• Complexity: 256

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC(=CC2=CC=CC=C21)C3=CC=CC=C3

Technology Process of 1-Methoxy-3-phenylnaphthalene

There total 12 articles about 1-Methoxy-3-phenylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

4-Methoxystyrene (637-69-4,24936-44-5) → 1-methoxy-3-phenylnaphthalene (59115-41-2) + 1-methoxy-4-((1RS,2SR)-2-phenylcyclopropyl)benzene (53400-00-3) + trans-1-(4-methoxyphenyl)-2-phenylcyclopropane (34221-26-6)

Guidance literature:

With Echavarren's catalyst; In dichloromethane; at 23 ℃; for 12h; optical yield given as %de; Inert atmosphere;

DOI:10.1021/ja104743k

Reference yield: 57.0%

1-(1-methoxyvinyl)-2-(phenylethynyl)benzene → 1-methoxy-3-phenylnaphthalene (59115-41-2) + 1-benzylidene-3-methoxy-1H-indene + 1-benzylidene-3-methoxy-1H-indene

Guidance literature:

With silver hexafluoroantimonate; chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I); In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/cjoc.202100582

Reference yield: 57.0%

1-(3-methoxy-3-(2-styrylphenyl)prop-1-ynyl)benzene → 1-methoxy-3-phenylnaphthalene (59115-41-2) + C31H26O

Guidance literature:

With Echavarren's catalyst; In dichloromethane; at 23 ℃; Inert atmosphere;

DOI:10.1021/ja104743k

upstream raw materials:

1,3-dimethoxynaphthalene

benzene

4-Methoxystyrene