Benzoic acid, 4-[bis[(diphenylphosphino)methyl]amino]-

Base Information

Chemical Name:Benzoic acid, 4-[bis[(diphenylphosphino)methyl]amino]-
CAS No.:592531-23-2
Molecular Formula:C33H29NO2P2
Molecular Weight:533.546
Hs Code.:
DSSTox Substance ID:DTXSID30406910
Nikkaji Number:J1.834.456D
Wikidata:Q82212055

Synonyms:592531-23-2;Benzoic acid, 4-[bis[(diphenylphosphino)methyl]amino]-;DTXSID30406910

Suppliers and Price of Benzoic acid, 4-[bis[(diphenylphosphino)methyl]amino]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 4-[bis[(diphenylphosphino)methyl]amino]-

Chemical Property:

XLogP3:7.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:10
Exact Mass:533.16735316
Heavy Atom Count:38
Complexity:609

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(CN(CP(C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=C(C=C4)C(=O)O)C5=CC=CC=C5

Technology Process of Benzoic acid, 4-[bis[(diphenylphosphino)methyl]amino]-

There total 2 articles about Benzoic acid, 4-[bis[(diphenylphosphino)methyl]amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 5958-44-1
diphenylphosphinomethanol

: 592531-23-2
4-{bis-[(diphenylphosphanyl)-methyl]-amino}-benzoic acid

Guidance literature:: In methanol; for 5.5h; Heating;
DOI:10.1016/S0040-4039(03)01273-5

Reference yield: 65.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 829-85-6
diphenylphosphane

: 592531-23-2
4-{bis-[(diphenylphosphanyl)-methyl]-amino}-benzoic acid

Guidance literature:: formaldehyd; diphenylphosphane; at 110 ℃; for 1h; Inert atmosphere; Schlenk technique;

4-amino-benzoic acid; In methanol; for 2h; Reflux; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.poly.2015.08.019

Reference yield: 94.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 592531-23-2
4-{bis-[(diphenylphosphanyl)-methyl]-amino}-benzoic acid

: 501337-97-9
PdCl₂(((C₆H₅)2PCH₂)2NC₆H₄CO₂H)

Guidance literature:: In dichloromethane; under N2; mixt. of ligand and Pd complex (molar ratio 1:1) in CH2Cl2 stirred at room temp. for 1 h; solvent evapd. slowly; washed with Et2O; elem. anal.;
DOI:10.1016/S0020-1693(02)00983-0