4H-1,3,2-Benzodioxaborin, 2,4-diphenyl-

Base Information

Chemical Name:4H-1,3,2-Benzodioxaborin, 2,4-diphenyl-
CAS No.:59648-27-0
Molecular Formula:C19H15BO2
Molecular Weight:286.138
Hs Code.:

Synonyms:

Suppliers and Price of 4H-1,3,2-Benzodioxaborin, 2,4-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 4H-1,3,2-Benzodioxaborin, 2,4-diphenyl-

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4H-1,3,2-Benzodioxaborin, 2,4-diphenyl-

There total 1 articles about 4H-1,3,2-Benzodioxaborin, 2,4-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 100-52-7
benzaldehyde

: 108-95-2,27073-41-2
phenol

: 98-80-6
phenylboronic acid

: 59648-27-0
2,4-diphenyl-1,3,2-benzodioxaborin

Guidance literature:: With aluminum oxide; for 0.25h; microwave irradiation;
DOI:10.1080/00397910600764741

Reference yield: 97.0%

: 59648-27-0
2,4-diphenyl-1,3,2-benzodioxaborin

: 28994-41-4
o-Benzylphenol

Guidance literature:: With aluminium trichloride; borane tert-butylamine; In dichloromethane; at 0 ℃; for 0.75h;

Reference yield: 97.0%

: 59648-27-0
2,4-diphenyl-1,3,2-benzodioxaborin

: borane tert-butylamine

: 28994-41-4
o-Benzylphenol

Guidance literature:: With aluminiumchloride; In dichloromethane; addn. of tert.-butylamine borane to suspn. of anhyd. AlCl3 at 0°C (20 min.), addn. of soln. of the 1,3,2-benzodioxaborin in CH2Cl2, allowed to react at 0°C for 45 min; addn. of cold dilute HCl; extn. with CH2Cl2, organic extracts dried over anhyd. MgSO4, concd., chromy. (silica gel, 10% ethyl acetate in hexane);