[hydrazino(dimethyl)silyl]hydrazine

Base Information

• Chemical Name: [hydrazino(dimethyl)silyl]hydrazine
• CAS No.: 6026-17-1
• Molecular Formula: C6H20N4Si
• Molecular Weight: 120.22900

Synonyms:N',N',N''',N'''-tetramethyl-N,N''-dimethylsilanediyl-bis-hydrazine;DIMETHYL 1,1'-BICYCLOHEXANEDICARBOXYLATE;2,2'-diindenyldimethylsilane;Dimethyl-bis--silan;Dimethyl-bicyclohexyl-1,1'-dicarboxylat;<1,1'-bicyclohexyl>-1,1'-dicarboxylic acid dimethyl ester;dimethylbisindenylsilane;

Chemical Property of [hydrazino(dimethyl)silyl]hydrazine

Chemical Property:

• Vapor Pressure: 2.655mmHg at 25°C
• Boiling Point: 158.206oC at 760 mmHg
• Flash Point: 49.482oC
• PSA: 76.10000
• Density: 0.983g/cm3
• LogP: 0.79720

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [hydrazino(dimethyl)silyl]hydrazine

There total 2 articles about [hydrazino(dimethyl)silyl]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

N,N-Dimethylhydrazine (57-14-7) + dimethylsilicon dichloride (75-78-5,30107-43-8) → bis(2,2-dimethylhydrazino)dimethylsilane (6026-17-1)

Guidance literature:

In diethyl ether; for 1h; Heating;

DOI:10.1023/A:1022527112583

Reference yield:

(N,N-diethylamino)dimethylchlorosilane (6026-02-4) + N,N-Dimethylhydrazine (57-14-7) → bis(2,2-dimethylhydrazino)dimethylsilane (6026-17-1)

Guidance literature:

In Petroleum ether; Heating;

DOI:10.1007/BF01185914

Reference yield:

bis(2,2-dimethylhydrazino)dimethylsilane (6026-17-1) + sec-Butyl-difluoro-methyl-silane → 2-sec-Butyl-2,4,4,N,N,N',N'-heptamethyl-[1,3,2,4]diazadisiletidine-1,3-diamine (66436-32-6)

Guidance literature:

Multistep reaction; (i) nBuLi, (ii) /BRN= 6693134/;

upstream raw materials:

(N,N-diethylamino)dimethylchlorosilane

N,N-Dimethylhydrazine

dimethylsilicon dichloride

Downstream raw materials:

2-sec-Butyl-2,4,4,N,N,N',N'-heptamethyl-[1,3,2,4]diazadisiletidine-1,3-diamine

2-Butyl-2-tert-butyl-4,4,N,N,N',N'-hexamethyl-[1,3,2,4]diazadisiletidine-1,3-diamine

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