3,5-Pyridinedicarboxylic acid, 2-[(2S)-1-[(1,1-dimethylethoxy)carbonyl]-2-pyrrolidinyl]-4-[6-(ethoxycarb onyl)-3-pyridazinyl]-6-[(4-fluorophenyl)methyl]-1,4-dihydro-, diethyl ester

Base Information

• Chemical Name: 3,5-Pyridinedicarboxylic acid, 2-[(2S)-1-[(1,1-dimethylethoxy)carbonyl]-2-pyrrolidinyl]-4-[6-(ethoxycarb onyl)-3-pyridazinyl]-6-[(4-fluorophenyl)methyl]-1,4-dihydro-, diethyl ester
• CAS No.: 604000-39-7
• Molecular Formula: C34H41FN4O8
• Molecular Weight: 652.72

Synonyms:

Chemical Property of 3,5-Pyridinedicarboxylic acid, 2-[(2S)-1-[(1,1-dimethylethoxy)carbonyl]-2-pyrrolidinyl]-4-[6-(ethoxycarb onyl)-3-pyridazinyl]-6-[(4-fluorophenyl)methyl]-1,4-dihydro-, diethyl ester

Chemical Property:

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Technology Process of 3,5-Pyridinedicarboxylic acid, 2-[(2S)-1-[(1,1-dimethylethoxy)carbonyl]-2-pyrrolidinyl]-4-[6-(ethoxycarb onyl)-3-pyridazinyl]-6-[(4-fluorophenyl)methyl]-1,4-dihydro-, diethyl ester

There total 1 articles about 3,5-Pyridinedicarboxylic acid, 2-[(2S)-1-[(1,1-dimethylethoxy)carbonyl]-2-pyrrolidinyl]-4-[6-(ethoxycarb onyl)-3-pyridazinyl]-6-[(4-fluorophenyl)methyl]-1,4-dihydro-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 6-formyl-3-pyridazinecarboxylate (604000-38-6) + ethyl-3-amino-4-(4-fluorophenyl)-2-butenoate (604000-41-1) + (S)-tert-butyl 2-(3-ethoxy-3-oxopropanoyl)pyrrolidine-1-carboxylate (109180-95-2,108310-01-6) → diethyl 2-[(2S)-1-(tert-butoxycarbonyl)pyrrolidinyl]-4-[6-(ethoxycarbonyl)-3-pyridazinyl]-6-(4-fluorobenzyl)-1,4-dihydro-3,5-pyridinedicarboxylate (604000-39-7)

Guidance literature:

With piperidine; acetic acid; In toluene; at 100 ℃; for 2h;

Reference yield:

diethyl 2-[(2S)-1-(tert-butoxycarbonyl)pyrrolidinyl]-4-[6-(ethoxycarbonyl)-3-pyridazinyl]-6-(4-fluorobenzyl)-1,4-dihydro-3,5-pyridinedicarboxylate (604000-39-7) → diethyl 2-[(2S)-1-(tert-butoxycarbonyl)pyrrolidinyl]-4-[6-(ethoxycarbonyl)-3-pyridazinyl]-6-(4-fluorobenzyl)-3,5-pyridinedicarboxylate (604000-43-3)

Guidance literature:

With ammonium cerium(IV) nitrate; In water; acetonitrile; for 0.0833333h;

upstream raw materials:

ethyl 6-formyl-3-pyridazinecarboxylate

ethyl-3-amino-4-(4-fluorophenyl)-2-butenoate

(S)-tert-butyl 2-(3-ethoxy-3-oxopropanoyl)pyrrolidine-1-carboxylate

Downstream raw materials:

diethyl 2-[(2S)-1-(tert-butoxycarbonyl)pyrrolidinyl]-4-[6-(ethoxycarbonyl)-3-pyridazinyl]-6-(4-fluorobenzyl)-3,5-pyridinedicarboxylate

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