2,6-DIPHENYLNAPHTHALENE

Base Information

• Chemical Name: 2,6-DIPHENYLNAPHTHALENE
• CAS No.: 60706-24-3
• Molecular Formula: C22H16
• Molecular Weight: 280.369
• Mol file: 60706-24-3.mol

Synonyms:2,6-Diphenyl-naphthalin;2,6-diphenyl-naphthalene;[Zn(mthd)2(bpy)];

Chemical Property of 2,6-DIPHENYLNAPHTHALENE

Chemical Property:

• PSA: 0.00000
• LogP: 6.17380

Purity/Quality:

99% ^*data from raw suppliers

2,6-DIPHENYLNAPHTHALENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-DIPHENYLNAPHTHALENE

There total 19 articles about 2,6-DIPHENYLNAPHTHALENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C23H18O3S (1247758-09-3) → [Zn(mthd)2(bpy)] (60706-24-3)

Guidance literature:

RLi or RMgBr, R = Ph; With indium(III) chloride; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

C₂₃H₁₈O₃S; With bis(tricyclohexylphosphine)nickel(II) dichloride; tricyclohexylphosphine; In tetrahydrofuran; at 20 - 80 ℃; Inert atmosphere;

DOI:10.1055/s-0030-1258116

Reference yield: 89.0%

C18H26O8P2 (1279101-98-2) + phenylboronic acid (98-80-6) → [Zn(mthd)2(bpy)] (60706-24-3)

Guidance literature:

With potassium phosphate; bis(tricyclohexylphosphine)nickel(II) dichloride; In 1,4-dioxane; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1021/jo2000034

Reference yield: 88.0%

N-trifluoromethanesulfony-6-phenyl-2-naphthalenamine + phenylmagnesium bromide (100-58-3) → [Zn(mthd)2(bpy)] (60706-24-3)

Guidance literature:

N-trifluoromethanesulfony-6-phenyl-2-naphthalenamine; phenylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Schlenk technique; Inert atmosphere;

With bis(tricyclohexylphosphine)nickel(II) dichloride; 1,3-di-cyclohexyl-4-methyl-benzimidazolium chloride; In toluene; butan-1-ol; at 70 ℃; for 12.03h; Schlenk technique; Inert atmosphere; Glovebox;

DOI:10.1021/acs.orglett.0c03660

upstream raw materials:

2,6-Dicyclohexylnaphthalene

2,6-Diphenyl-1,2-dihydro-naphthalene

phenylmagnesium bromide

6-bromo-2-naphthalenyl trifluoromethanesulfonate