Technology Process of 2-Propanol, 1-(octadecyloxy)-3-(triphenylmethoxy)-, (S)-
There total 13 articles about 2-Propanol, 1-(octadecyloxy)-3-(triphenylmethoxy)-, (S)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
Ru2Cl4{(R)-binap}2(C2H5)3N;
In
dichloromethane;
at 20 ℃;
for 96h;
under 73580.8 Torr;
DOI:10.1016/S0040-4039(00)92176-2
- Guidance literature:
-
Multi-step reaction with 6 steps
1: toluene / 1 h / 80 °C
2: pyridine / CHCl3 / Ambient temperature
3: H2 / 5percent Pd/C / tetrahydrofuran / Ambient temperature
4: phosphorus oxychloride, Et3N, pyridine / CHCl3 / Ambient temperature
5: 66 percent / LiAlH4 / tetrahydrofuran / Ambient temperature
6: 81 percent / pyridine / Ambient temperature
With
pyridine; lithium aluminium tetrahydride; hydrogen; triethylamine; trichlorophosphate;
palladium on activated charcoal;
In
tetrahydrofuran; chloroform; toluene;
DOI:10.1002/hlca.19820650339
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium chlorochromate / CH2Cl2
2: 70 percent / H2 / 2Cl4-((R)-bis(diphenylphosphino-1,1'-binaphthalene)2>NEt3 (Ru(R)BINAP) / CH2Cl2 / 96 h / 20 °C / 73580.8 Torr
With
hydrogen; pyridinium chlorochromate;
Ru2Cl4{(R)-binap}2(C2H5)3N;
In
dichloromethane;
DOI:10.1016/S0040-4039(00)92176-2
