4-(4-Methoxyphenyl)-1H-2,3-benzoxazin-1-one

Base Information

• Chemical Name: 4-(4-Methoxyphenyl)-1H-2,3-benzoxazin-1-one
• CAS No.: 65441-03-4
• Molecular Formula: C15H11 N O3
• Molecular Weight: 253.257
• Hs Code.: 2934999090
• Mol file: 65441-03-4.mol

Synonyms:1H-2,3-Benzoxazin-1-one,4-(p-methoxyphenyl)- (6CI,7CI); NSC 303584

Chemical Property of 4-(4-Methoxyphenyl)-1H-2,3-benzoxazin-1-one

Chemical Property:

• Vapor Pressure: 4.58E-07mmHg at 25°C
• Melting Point: 141 °C
• Boiling Point: 414.1°C at 760 mmHg
• Flash Point: 196.8°C
• PSA: 52.33000
• Density: 1.24g/cm³
• LogP: 2.86360

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(4-Methoxyphenyl)-1H-2,3-benzoxazin-1-one

There total 3 articles about 4-(4-Methoxyphenyl)-1H-2,3-benzoxazin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(4-methoxy-phenyl)-3,4-dihydro-1H-benzo[d][1,2]oxazin-1-ol (72873-55-3) → 4-(4-methoxy-phenyl)-2,3-benzoxazin-1-one (65441-03-4)

Guidance literature:

With potassium dichromate; sulfuric acid; In diethyl ether;

Reference yield:

2-(4-methoxybenzoyl)benzoic acid (1151-15-1) → 4-(4-methoxy-phenyl)-2,3-benzoxazin-1-one (65441-03-4)

Guidance literature:

With hydrogenchloride; hydroxylamine;

Reference yield:

→ 4-(4-methoxy-phenyl)-2,3-benzoxazin-1-one (65441-03-4)

Guidance literature:

o-Anisoyl-benzazid (Ic), NH2OH/HCl (S.226);

upstream raw materials:

2-(4-methoxybenzoyl)benzoic acid

4-(4-methoxy-phenyl)-3,4-dihydro-1H-benzo[d][1,2]oxazin-1-ol

Downstream raw materials:

tetraethyl 1-(4-methoxyphenyl)-4-thioxo-3,4-dihydroisoquinoline-3,3-diyldiphosphonate

4-(4-methoxyphenyl)-1H-2,3-benzothiazine-1-thione

3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat

3-Methoxy-1-(4-methoxyphenyl)-1H-isoindol

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