Technology Process of CID 53959807
There total 6 articles about CID 53959807 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
trimethylsilyl acetate; 3-phenyl-propenal;
With
trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
With
water; trifluoroacetic acid;
In
ethanol; dichloromethane;
Inert atmosphere;
DOI:10.1021/jo100828c
- Guidance literature:
-
acetic acid; 3-phenyl-propenal;
With
trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
With
water; trifluoroacetic acid;
In
ethanol; dichloromethane;
Inert atmosphere;
DOI:10.1021/jo100828c
- Guidance literature:
-
With
sodium hydroxide;
In
ethanol; water;
at 20 ℃;
for 3h;
DOI:10.1039/d0cc05630h
