2-Propenoic acid, 3-(benzoylamino)-, methyl ester, (E)-

Base Information

Chemical Name:2-Propenoic acid, 3-(benzoylamino)-, methyl ester, (E)-
CAS No.:62183-16-8
Molecular Formula:C11H11NO3
Molecular Weight:205.213
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propenoic acid, 3-(benzoylamino)-, methyl ester, (E)-

Chemical Property:

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Technology Process of 2-Propenoic acid, 3-(benzoylamino)-, methyl ester, (E)-

There total 9 articles about 2-Propenoic acid, 3-(benzoylamino)-, methyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: methyl (E)-3-(N-(tert-butoxycarbonyl)benzamido)acrylate

: 62183-16-8
methyl (E)-3-benzamidoacrylate

Guidance literature:: With magnesium(II) perchlorate; In acetonitrile; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/acs.joc.1c01212

Reference yield: 75.0%

: 89928-06-3
methyl ester of 3-(N-benzoyl)aminopropionic acid

: 62183-16-8
methyl (E)-3-benzamidoacrylate

Guidance literature:: methyl ester of 3-(N-benzoyl)aminopropionic acid; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -40 ℃; for 1h; Inert atmosphere;

With zinc(II) chloride; In tetrahydrofuran; 2-methyltetrahydrofuran; hexane; at -40 ℃; for 1h; Inert atmosphere;

With bis(η3-allyl-μ-chloropalladium(II)); Allyl acetate; In tetrahydrofuran; 2-methyltetrahydrofuran; hexane; at -40 - 60 ℃; for 12h; chemoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2018.02.028

Reference yield: 50.0%

: 55-21-0,27208-38-4
benzamide

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 62183-17-9
(Z)-methyl 3-(benzamido)acrylate

: 62183-16-8
methyl (E)-3-benzamidoacrylate

Guidance literature:: With silver(I) acetate; palladium diacetate; In 1,4-dioxane; at 20 ℃; for 48h; Reagent/catalyst; Temperature; regioselective reaction; Sealed tube;
DOI:10.1021/acs.joc.7b00966