2-Propynal, 3-(3-methylphenyl)-

Base Information

Chemical Name:2-Propynal, 3-(3-methylphenyl)-
CAS No.:62358-91-2
Molecular Formula:C10H8O
Molecular Weight:144.173
Hs Code.:

Synonyms:1-(3-toluyl)-2-propyn-1-al;3-(3-methylphenyl)propynal;m-tolylpropynal;3-(3-methylphenyl)-2-propynaldehyde;3-m-tolylpropiolaldehyde;3-(m-tolyl)propiolaldehyde;m-Tolyl-propynal;

Suppliers and Price of 2-Propynal, 3-(3-methylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Propynal, 3-(3-methylphenyl)-

Chemical Property:

PSA：17.07000
LogP:1.54540

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Propynal, 3-(3-methylphenyl)-

There total 11 articles about 2-Propynal, 3-(3-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 97065-56-0
1-(2,2-dibromovinyl)-3-methylbenzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 62358-91-2
3-(3-methylphenyl)prop-2-ynal

Guidance literature:: 1-(2,2-dibromovinyl)-3-methylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -50 - -40 ℃; for 0.25h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -40 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c4cc09495f

Reference yield: 82.0%

: 16035-11-3
3-(3-methylphenyl)propargyl alcohol

: 62358-91-2
3-(3-methylphenyl)prop-2-ynal

Guidance literature:: 3-(3-methylphenyl)propargyl alcohol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.25h;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 0.833333h;
DOI:10.1002/adsc.201800305

Reference yield: 48.0%

: 20461-86-3
2,2-diethoxy acetic acid

: 33675-43-3
1-(bromo-ethynyl)-3-methyl-benzene

: 62358-91-2
3-(3-methylphenyl)prop-2-ynal

Guidance literature:: With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; caesium carbonate; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃; for 24h; Irradiation; Inert atmosphere;
DOI:10.1039/c9ra06596b