4-(Benzyloxy)picolinaldehyde

Base Information

Chemical Name:4-(Benzyloxy)picolinaldehyde
CAS No.:63071-14-7
Molecular Formula:C13H11NO2
Molecular Weight:213.236
Hs Code.:2933399090
DSSTox Substance ID:DTXSID50489467

Synonyms:4-(Benzyloxy)picolinaldehyde;63071-14-7;4-Phenylmethoxypyridine-2-carbaldehyde;4-(Benzyloxy)pyridine-2-carbaldehyde;SCHEMBL19859637;DTXSID50489467;MFCD18256122;AKOS016000866;s11424;AS-62858;CS-0060547;A868254

Suppliers and Price of 4-(Benzyloxy)picolinaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-(Benzyloxy)picolinaldehyde 95%
1g
$ 583.00

Chemenu
4-(Benzyloxy)picolinaldehyde 97%
1g
$ 482.00

American Custom Chemicals Corporation
4-(BENZYLOXY)PICOLINALDEHYDE 95.00%
5MG
$ 499.29

AK Scientific
4-(Benzyloxy)picolinaldehyde
100mg
$ 236.00

Total 15 raw suppliers

Chemical Property of 4-(Benzyloxy)picolinaldehyde

Chemical Property:

Melting Point:89.5 °C
Boiling Point:125-128 °C(Press: 0.02 Torr)
PKA:4.43±0.10(Predicted)
PSA：39.19000
Density:1.191±0.06 g/cm3(Predicted)
LogP:2.47310
Storage Temp.:Inert atmosphere,Store in freezer, under -20°C
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:213.078978594
Heavy Atom Count:16
Complexity:214

Purity/Quality:

97% ^*data from raw suppliers

4-(Benzyloxy)picolinaldehyde 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=CC(=NC=C2)C=O

Technology Process of 4-(Benzyloxy)picolinaldehyde

There total 10 articles about 4-(Benzyloxy)picolinaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.8%

: 4-(benzyloxy)-N-methoxy-N-methylpicolinamide

: 63071-14-7
4-(benzyloxy)pyridine-2-carbaldehyde

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 1.5h; Inert atmosphere;

Reference yield:

: 63071-11-4
4-(benzyloxy)-2-(hydroxymethyl)pyridine

: 63071-14-7
4-(benzyloxy)pyridine-2-carbaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 1.5h;

Reference yield:

: 100727-49-9
4-(benzyloxy)picolinic acid

: 63071-14-7
4-(benzyloxy)pyridine-2-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0.25 h / 0 - 20 °C

1.2: 20 °C

2.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1.5 h / -78 °C / Inert atmosphere

With diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;