2,4-Pyrimidinediamine,5-[4-chloro-3-(3,3-dimethyl-1-triazen-1-yl)phenyl]-6-ethyl-

Base Information

Chemical Name:2,4-Pyrimidinediamine,5-[4-chloro-3-(3,3-dimethyl-1-triazen-1-yl)phenyl]-6-ethyl-
CAS No.:113494-48-7
Molecular Formula:C₁₄H₁₈ClN₇
Molecular Weight:319.797
Hs Code.:
Mol file:113494-48-7.mol

Synonyms:2,4-Pyrimidinediamine,5-[4-chloro-3-(3,3-dimethyl-1-triazenyl)phenyl]-6-ethyl- (9CI); NSC 330465

Suppliers and Price of 2,4-Pyrimidinediamine,5-[4-chloro-3-(3,3-dimethyl-1-triazen-1-yl)phenyl]-6-ethyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-Pyrimidinediamine,5-[4-chloro-3-(3,3-dimethyl-1-triazen-1-yl)phenyl]-6-ethyl-

Chemical Property:

Boiling Point:564.2°Cat760mmHg
Flash Point:295°C
Density:1.38g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4-Pyrimidinediamine,5-[4-chloro-3-(3,3-dimethyl-1-triazen-1-yl)phenyl]-6-ethyl-

There total 5 articles about 2,4-Pyrimidinediamine,5-[4-chloro-3-(3,3-dimethyl-1-triazen-1-yl)phenyl]-6-ethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58-14-0
2,4-diamino-5-(4-chlorophenyl)-6-ethylpyrimidine

: 113494-48-7
2,4-diamino-5-<4-chloro-3-(3,3-dimethyltriazen-1-yl)phenyl>-6-ethylpyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / nitric acid (d=1.42), cc. H₂SO₄ / 1 h / 50 °C

2: SnCl₂*2H₂O / ethanol / Heating

3: 1.) 3M aq. HCl, aq. NaNO₂ / 1.) 0 deg C; 2.) 0 deg C, 2 h

With hydrogenchloride; sulfuric acid; nitric acid; tin(ll) chloride; sodium nitrite; In ethanol;
DOI:10.1039/P19870002217

Reference yield:

: 21813-35-4
2,4-diamino-5-(4-chloro-3-nitrophenyl)-6-ethylpyrimidine

: 113494-48-7
2,4-diamino-5-<4-chloro-3-(3,3-dimethyltriazen-1-yl)phenyl>-6-ethylpyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: SnCl₂*2H₂O / ethanol / Heating

2: 1.) 3M aq. HCl, aq. NaNO₂ / 1.) 0 deg C; 2.) 0 deg C, 2 h

With hydrogenchloride; tin(ll) chloride; sodium nitrite; In ethanol;
DOI:10.1039/P19870002217

Reference yield:

: 95458-40-5
2,4-diamino-5-(3-azido-4-chlorophenyl)-6-ethylpyrimidine

: 113494-48-7
2,4-diamino-5-<4-chloro-3-(3,3-dimethyltriazen-1-yl)phenyl>-6-ethylpyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: NaHS / H₂O / 65 °C

2: 1.) 3M aq. HCl, aq. NaNO₂ / 1.) 0 deg C; 2.) 0 deg C, 2 h

With hydrogenchloride; sodium hydrogensulfide; sodium nitrite; In water;
DOI:10.1039/P19870002217