3'-Adenylic acid, N-(4-methoxybenzoyl)-2'-O-(tetrahydro-4-methoxy-2H-pyran-4-yl)-, 2-chlorophenyl 2,2,2-trichloroethyl ester, 5'-(4-oxopentanoate)

Base Information

Chemical Name:3'-Adenylic acid, N-(4-methoxybenzoyl)-2'-O-(tetrahydro-4-methoxy-2H-pyran-4-yl)-, 2-chlorophenyl 2,2,2-trichloroethyl ester, 5'-(4-oxopentanoate)
CAS No.:63358-76-9
Molecular Formula:C₃₇H₄₀Cl₄N₅O₁₃P
Molecular Weight:935.536
Hs Code.:

3'-Adenylic acid,
N-(4-methoxybenzoyl)-2'-O-(tetrahydro-4-methoxy-2H-pyran-4-yl)-,
2-chlorophenyl 2,2,2-trichloroethyl ester, 5'-(4-oxopentanoate)

Synonyms:

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Chemical Property of 3'-Adenylic acid, N-(4-methoxybenzoyl)-2'-O-(tetrahydro-4-methoxy-2H-pyran-4-yl)-, 2-chlorophenyl 2,2,2-trichloroethyl ester, 5'-(4-oxopentanoate)

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Technology Process of 3'-Adenylic acid, N-(4-methoxybenzoyl)-2'-O-(tetrahydro-4-methoxy-2H-pyran-4-yl)-, 2-chlorophenyl 2,2,2-trichloroethyl ester, 5'-(4-oxopentanoate)

There total 4 articles about 3'-Adenylic acid, N-(4-methoxybenzoyl)-2'-O-(tetrahydro-4-methoxy-2H-pyran-4-yl)-, 2-chlorophenyl 2,2,2-trichloroethyl ester, 5'-(4-oxopentanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 59819-52-2
2,2,2-trichloroethyl 2-chlorophenyl phosphorochloridate

: 69497-76-3
4-Oxo-pentanoic acid (2R,3R,4R,5R)-3-hydroxy-5-[6-(4-methoxy-benzoylamino)-purin-9-yl]-4-(4-methoxy-tetrahydro-pyran-4-yloxy)-tetrahydro-furan-2-ylmethyl ester

: 63358-76-9
N⁶-(4-methoxy-benzoyl)-O^2'-(4-methoxy-tetrahydro-pyran-4-yl)-O^5'-(4-oxo-pentanoyl)-[3']adenylic acid 2-chloro-phenyl ester 2,2,2-trichloroethyl ester

Guidance literature:: With 1-methyl-1H-imidazole; In acetonitrile;

Reference yield:

: 60943-91-1
N⁶-(4-methoxy-benzoyl)-O^2'-(4-methoxy-tetrahydro-pyran-4-yl)-adenosine

: 63358-76-9
N⁶-(4-methoxy-benzoyl)-O^2'-(4-methoxy-tetrahydro-pyran-4-yl)-O^5'-(4-oxo-pentanoyl)-[3']adenylic acid 2-chloro-phenyl ester 2,2,2-trichloroethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 2-chloro-1-methylpyridinium iodide, 1,4-diazabicyclo<2.2.2>octane / acetonitrile; dioxane / 2 h

2: 83 percent / 1-methylimidazole / acetonitrile

With 1,4-diaza-bicyclo[2.2.2]octane; 1-methyl-1H-imidazole; 2-chloro-1-methyl-pyridinium iodide; In 1,4-dioxane; acetonitrile;

Reference yield:

: 123-76-2
levulinic acid

: 63358-76-9
N⁶-(4-methoxy-benzoyl)-O^2'-(4-methoxy-tetrahydro-pyran-4-yl)-O^5'-(4-oxo-pentanoyl)-[3']adenylic acid 2-chloro-phenyl ester 2,2,2-trichloroethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 2-chloro-1-methylpyridinium iodide, 1,4-diazabicyclo<2.2.2>octane / acetonitrile; dioxane / 2 h

2: 83 percent / 1-methylimidazole / acetonitrile

With 1,4-diaza-bicyclo[2.2.2]octane; 1-methyl-1H-imidazole; 2-chloro-1-methyl-pyridinium iodide; In 1,4-dioxane; acetonitrile;