(4-ETHOXY-PHENYL)-OXO-ACETALDEHYDE

Base Information

• Chemical Name: (4-ETHOXY-PHENYL)-OXO-ACETALDEHYDE
• CAS No.: 14333-52-9
• Molecular Formula: C10H10 O3
• Molecular Weight: 178.188
• Hs Code.: 2914509090
• Mol file: 14333-52-9.mol

Synonyms:Glyoxal,(p-ethoxyphenyl)- (8CI); (4-Ethoxyphenyl)glyoxal; (p-Ethoxyphenyl)glyoxal; NSC400603

Chemical Property of (4-ETHOXY-PHENYL)-OXO-ACETALDEHYDE

Chemical Property:

• Vapor Pressure: 0.00372mmHg at 25°C
• Boiling Point: 280.7°Cat760mmHg
• Flash Point: 121.3°C
• PSA: 43.37000
• Density: 1.122g/cm³
• LogP: 1.46690

Purity/Quality:

98%min ^*data from raw suppliers

(4-Ethoxy-phenyl)-oxo-acetaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4-ETHOXY-PHENYL)-OXO-ACETALDEHYDE

There total 2 articles about (4-ETHOXY-PHENYL)-OXO-ACETALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4'-ethoxyacetophenone (1676-63-7) → (4-ethoxy-phenyl)-glyoxal (14333-52-9)

Guidance literature:

With tris(2,2'-bipyridyl)ruthenium dichloride; dioxane dibromide; sodium L-ascorbate; In acetonitrile; at 20 ℃; for 8h; Irradiation; Green chemistry;

DOI:10.1016/j.tetlet.2017.01.013

Reference yield:

1-(4-ethoxyphenyl)-2-iodoethanone (18276-98-7) → (4-ethoxy-phenyl)-glyoxal (14333-52-9)

Guidance literature:

With iodine; potassium hydroxide; In water; dimethyl sulfoxide; at 100 ℃;

DOI:10.1021/jo302754c

Reference yield: 85.0%

(4-ethoxy-phenyl)-glyoxal (14333-52-9) + monophenylthiourea (103-85-5) → 5-(4-ethoxyphenyl)-1-phenylthiohydantoin

Guidance literature:

With polyphosphoric ester; for 0.05h; microwave irradiation;

DOI:10.1055/s-2002-19308

upstream raw materials:

4'-ethoxyacetophenone

1-(4-ethoxyphenyl)-2-iodoethanone

Downstream raw materials:

2-(4-ethoxy-phenyl)-quinoxaline

2-(4'-ethoxyphenyl)-3-methoxy-6-(2-methoxyphenoxy)imidazo<1,2-b>pyridazine

C₁₄H₁₆N₂O₃

(4-ethoxyphenyl)-[5-(4-ethoxyphenyl)-1H-imidazol-2-yl]methanone

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