Technology Process of 1H-Inden-1-one, 2,3-dihydro-3-phenyl-, (3S)-
There total 32 articles about 1H-Inden-1-one, 2,3-dihydro-3-phenyl-, (3S)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
nickel(II) bromide dimethoxyethane; manganese; C36H49N3O2; water; lithium carbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 80 ℃;
for 24h;
enantioselective reaction;
Inert atmosphere;
Glovebox;
Schlenk technique;
DOI:10.1021/acs.orglett.9b02130
- Guidance literature:
-
phenylboronic acid;
With
bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; triethylamine;
In
1,4-dioxane; water;
at 20 ℃;
for 2h;
Inert atmosphere;
1H-inden-1-one;
In
1,4-dioxane; water;
at 100 ℃;
for 4h;
enantioselective reaction;
Inert atmosphere;
DOI:10.1055/s-0030-1260823
- Guidance literature:
-
With
indium(III) triflate; isopropyl alcohol;
In
hexane;
at 150 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/ja909669e
