Benzeneacetonitrile, a-(3-methyl-1-oxobutyl)-

Base Information

Chemical Name:Benzeneacetonitrile, a-(3-methyl-1-oxobutyl)-
CAS No.:634199-47-6
Molecular Formula:C13H15NO
Molecular Weight:201.268
Hs Code.:

Synonyms:

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Chemical Property of Benzeneacetonitrile, a-(3-methyl-1-oxobutyl)-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzeneacetonitrile, a-(3-methyl-1-oxobutyl)-

There total 1 articles about Benzeneacetonitrile, a-(3-methyl-1-oxobutyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 556-24-1
methyl 3-methylbutanoate

: 140-29-4
phenylacetonitrile

: 634199-47-6
5-methyl-3-oxo-2-phenyl-hexanenitrile

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 85 ℃; for 21h;
DOI:10.1081/SCC-120024725

Reference yield:

: 634199-47-6
5-methyl-3-oxo-2-phenyl-hexanenitrile

: 634199-55-6
5-(4'-aminophenyl)-6-isobutyl-pyrimidine-2,4-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: conc. H₂SO₄; molecular sieves / 18 h / 180 - 200 °C

2: 25 percent / NaOEt / ethanol / 8 h / 130 °C

3: 35 percent / conc. H₂SO₄; conc. HNO₃ / 2 h / 0 - 20 °C

4: 99 percent / H₂ / Raney nickel / methanol; tetrahydrofuran / 18 h / 2585.74 Torr

With molecular sieve; sulfuric acid; hydrogen; nitric acid; sodium ethanolate; nickel; In tetrahydrofuran; methanol; ethanol;
DOI:10.1081/SCC-120024725

Reference yield:

: 634199-47-6
5-methyl-3-oxo-2-phenyl-hexanenitrile

: 634199-50-1
6-isobutyl-5-(4'-nitrophenyl)-pyrimidine-2,4-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: conc. H₂SO₄; molecular sieves / 18 h / 180 - 200 °C

2: 25 percent / NaOEt / ethanol / 8 h / 130 °C

3: 35 percent / conc. H₂SO₄; conc. HNO₃ / 2 h / 0 - 20 °C

With molecular sieve; sulfuric acid; nitric acid; sodium ethanolate; In ethanol;
DOI:10.1081/SCC-120024725