Phosphinic amide, N-ethyl-P,P-diphenyl-

Base Information

Chemical Name:Phosphinic amide, N-ethyl-P,P-diphenyl-
CAS No.:63528-17-6
Molecular Formula:C14H16NOP
Molecular Weight:245.261
Hs Code.:
DSSTox Substance ID:DTXSID00364093
Nikkaji Number:J1.572.879E
Wikidata:Q82147860

Synonyms:Phosphinic amide, N-ethyl-P,P-diphenyl-;63528-17-6;N-Ethyldiphenylphosphinamide;DTXSID00364093

Suppliers and Price of Phosphinic amide, N-ethyl-P,P-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphinic amide, N-ethyl-P,P-diphenyl-

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:245.096951132
Heavy Atom Count:17
Complexity:245

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCNP(=O)(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of Phosphinic amide, N-ethyl-P,P-diphenyl-

There total 5 articles about Phosphinic amide, N-ethyl-P,P-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 557-66-4
ethanamine hydrochloride

: 4559-70-0
Diphenylphosphine oxide

: 63528-17-6
N-ethyl-P,P-diphenylphosphinic amide

Guidance literature:: With tetrachloromethane; sodium hydroxide; In dichloromethane; water; at 0 - 25 ℃;
DOI:10.1007/s11172-009-0256-3

Reference yield: 80.0%

: 64-17-5
ethanol

: 5994-87-6
diphenylphosphinamide

: 63528-17-6
N-ethyl-P,P-diphenylphosphinic amide

Guidance literature:: With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)-amino]ruthenium(II); potassium hydroxide; In toluene; at 110 ℃; for 16h; Inert atmosphere; Sealed tube; Glovebox;
DOI:10.1016/j.tet.2019.04.029

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 63528-17-6
N-ethyl-P,P-diphenylphosphinic amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: water / benzene / 20 - 30 °C

1.2: pH 8 - 9

2.1: tetrachloromethane; sodium hydroxide / dichloromethane; water / 0 - 25 °C

With tetrachloromethane; water; sodium hydroxide; In dichloromethane; water; benzene; 2.1: Todd-Atherton reaction;
DOI:10.1007/s11172-009-0256-3