6-But-3-enyl-1,5-dimethoxycyclohexa-1,4-diene

Base Information

Chemical Name:6-But-3-enyl-1,5-dimethoxycyclohexa-1,4-diene
CAS No.:63588-96-5
Molecular Formula:C12H18O2
Molecular Weight:194.274
Hs Code.:
DSSTox Substance ID:DTXSID00495937

Synonyms:6-but-3-enyl-1,5-dimethoxycyclohexa-1,4-diene;63588-96-5;DTXSID00495937;6-(3-butenyl)-1,5-dimethoxy-1,4-cyclohexadiene;6-(But-3-en-1-yl)-1,5-dimethoxycyclohexa-1,4-diene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-But-3-enyl-1,5-dimethoxycyclohexa-1,4-diene

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:194.130679813
Heavy Atom Count:14
Complexity:231

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CCC=C(C1CCC=C)OC

Technology Process of 6-But-3-enyl-1,5-dimethoxycyclohexa-1,4-diene

There total 2 articles about 6-But-3-enyl-1,5-dimethoxycyclohexa-1,4-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5162-44-7
1-bromo-4-butene

: 37567-78-5
1,5-dimethoxy-1,4-cyclohexadiene

: 63588-96-5
6-(but-3-en-1-yl)-1,5-dimethoxycyclohexa-1,4-diene

Guidance literature:: 1,5-dimethoxy-1,4-cyclohexadiene; With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere; Schlenk technique;

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; at -78 ℃; Inert atmosphere; Schlenk technique;

1-bromo-4-butene; In tetrahydrofuran; at -78 - 20 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.7b00836

Reference yield:

: 63588-96-5
6-(but-3-en-1-yl)-1,5-dimethoxycyclohexa-1,4-diene

Guidance literature:: Verb. (3), 4-Brom-1-Buten;
DOI:10.1021/jo00443a029

Reference yield: 100.0%

: 63588-96-5
6-(but-3-en-1-yl)-1,5-dimethoxycyclohexa-1,4-diene

: 56459-16-6
2-(but-3-en-1-yl)cyclohexane-1,3-dione

Guidance literature:: With hydrogenchloride; In water; acetone; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.7b00836