Ethanone, 1-[3,4,6-trimethoxy-2-(1-methylethoxy)phenyl]-

Base Information

Chemical Name:Ethanone, 1-[3,4,6-trimethoxy-2-(1-methylethoxy)phenyl]-
CAS No.:63635-42-7
Molecular Formula:C14H20O5
Molecular Weight:268.31
Hs Code.:
DSSTox Substance ID:DTXSID80441836
Nikkaji Number:J819.310J
Wikidata:Q82258805

Synonyms:63635-42-7;Ethanone, 1-[3,4,6-trimethoxy-2-(1-methylethoxy)phenyl]-;DTXSID80441836;2'-Isopropoxy-3',4',6'-trimethoxyacetophenone

Suppliers and Price of Ethanone, 1-[3,4,6-trimethoxy-2-(1-methylethoxy)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Ethanone, 1-[3,4,6-trimethoxy-2-(1-methylethoxy)phenyl]-

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:268.13107373
Heavy Atom Count:19
Complexity:292

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)OC1=C(C(=CC(=C1OC)OC)OC)C(=O)C

Technology Process of Ethanone, 1-[3,4,6-trimethoxy-2-(1-methylethoxy)phenyl]-

There total 7 articles about Ethanone, 1-[3,4,6-trimethoxy-2-(1-methylethoxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1392322-52-9
1-isopropoxy-2,3,5-trimethoxybenzene

: 75-36-5
acetyl chloride

: 1392322-53-0
1-(4-isopropoxy-2,3,6-trimethoxyphenyl)ethanone

: 63635-42-7
1-(2-isopropoxy-3,4,6-trimethoxyphenyl)ethanone

Guidance literature:: With tin(IV) chloride; In dichloromethane; at 20 ℃;
DOI:10.1248/cpb.60.557

Reference yield:

: C₁₁H₁₆O₄

: 1392322-53-0
1-(4-isopropoxy-2,3,6-trimethoxyphenyl)ethanone

: 63635-42-7
1-(2-isopropoxy-3,4,6-trimethoxyphenyl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / methanol / 48 h / 20 °C

2: tin(IV) chloride / dichloromethane / 20 °C

With tin(IV) chloride; potassium hydroxide; In methanol; dichloromethane; 2: Friedel Crafts acylation;
DOI:10.1248/cpb.60.557

Reference yield:

: 195506-21-9
3-isopropoxy-4,5-dimethoxybenzaldehyde

: 1392322-53-0
1-(4-isopropoxy-2,3,6-trimethoxyphenyl)ethanone

: 63635-42-7
1-(2-isopropoxy-3,4,6-trimethoxyphenyl)ethanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C

1.2: 2 h / 20 °C

2.1: potassium hydroxide / methanol / 48 h / 20 °C

3.1: tin(IV) chloride / dichloromethane / 20 °C

With tin(IV) chloride; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In methanol; dichloromethane; 1.1: Baeyer-Villiger oxidation / 3.1: Friedel Crafts acylation;
DOI:10.1248/cpb.60.557