Germane, bis(methylthio)diphenyl-

Base Information

Chemical Name:Germane, bis(methylthio)diphenyl-
CAS No.:3860-83-1
Molecular Formula:C14H16GeS2
Molecular Weight:321.003
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germane, bis(methylthio)diphenyl-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Germane, bis(methylthio)diphenyl-

There total 12 articles about Germane, bis(methylthio)diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 624-92-0
Dimethyldisulphide

: 7366-24-7
phenyldichlorogermane

: 3860-83-1
bis(methy1thio)diphenylgermane

Guidance literature:: With triethylamine; In benzene; byproducts: (C2H5)3NHCl; Et3N adding in excess to germane soln. in benzene, stirring at ambient temp., Et3NHCl filtering off, ligand adding, heating in a sealed tube for 3 h at 100°C;
DOI:10.1016/S0022-328X(00)87639-1

Reference yield: 76.0%

: 624-92-0
Dimethyldisulphide

: 7366-23-6
diphenylchlorogermane

: 3860-83-1
bis(methy1thio)diphenylgermane

Guidance literature:: With triethylamine; In benzene; disulfide adding to a soln. of germylene complex freshly prepared by action of Et3N to Ph2GeHCl, heating for 4 h at 120 degree.C in a sealed tube; detd. by chromy. and NMR spectrum;
DOI:10.1016/0022-328X(84)85145-1

Reference yield: 52.0%

: tetraphenyldigermylmercury

: 624-92-0
Dimethyldisulphide

: 3860-83-1
bis(methy1thio)diphenylgermane

: 91123-33-0
(C₆H₅)2Ge(SCH₃)Ge(SCH₃)(C₆H₅)2

: 68816-03-5
diphenylgermylene

: mercury

Guidance literature:: In benzene; Irradiation (UV/VIS); disulfide adding to a soln. of Hg deriv., urradiating for 1 h; identified by chromy. and NMR spectrum;
DOI:10.1016/0022-328X(84)85145-1