2-(1,3-Dioxolan-2-yl)-4-methoxyaniline

Base Information

Chemical Name:2-(1,3-Dioxolan-2-yl)-4-methoxyaniline
CAS No.:64389-34-0
Molecular Formula:C10H13NO3
Molecular Weight:195.218
Hs Code.:
DSSTox Substance ID:DTXSID00571720
Wikidata:Q82459882

Synonyms:2-(1,3-Dioxolan-2-yl)-4-methoxyaniline;64389-34-0;SCHEMBL2469533;DTXSID00571720;NYAIQVOYPPYQIG-UHFFFAOYSA-N;2-(1,3-dioxolan-2yl)-4-methoxyphenylamine;2-(1,3-dioxolan-2-yl)-4-methoxyphenylamine

Suppliers and Price of 2-(1,3-Dioxolan-2-yl)-4-methoxyaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(1,3-Dioxolan-2-yl)-4-methoxyaniline

Chemical Property:

XLogP3:0.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:195.08954328
Heavy Atom Count:14
Complexity:182

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)N)C2OCCO2

Technology Process of 2-(1,3-Dioxolan-2-yl)-4-methoxyaniline

There total 3 articles about 2-(1,3-Dioxolan-2-yl)-4-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 73428-02-1
5-methoxy-2-nitrobenzaldehyde ethylene acetal

: 64389-34-0
5-methoxy-2-aminobenzaldehyde ethylene acetal

Guidance literature:: With hydrogen; sodium acetate; platinum(IV) oxide; In ethyl acetate; for 16h; under 3345.86 Torr;

Reference yield:

: 20357-24-8
5-methoxy-2-nitro-benzaldehyde

: 64389-34-0
5-methoxy-2-aminobenzaldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / p-toluenesul;fonic acid / toluene / 6 h / Heating

2: 89 percent / sodium sulfide / ethanol; H₂O / 0.5 h / Heating

With sodium sulfide; toluene-4-sulfonic acid; In ethanol; water; toluene;
DOI:10.1021/jm00179a016

Reference yield:

: 42454-06-8
2-nitro-5-hydroxybenzaldehyde

: 64389-34-0
5-methoxy-2-aminobenzaldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: toluene-4-sulfonic acid / toluene / 100 °C

3: platinum(IV) oxide; hydrogen; sodium acetate / ethyl acetate / 20 °C

With platinum(IV) oxide; hydrogen; sodium acetate; potassium carbonate; toluene-4-sulfonic acid; In ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2011.12.112