Desamino (αS)-Chloro Histidine Methyl Ester

Base Information

• Chemical Name: Desamino (αS)-Chloro Histidine Methyl Ester
• CAS No.: 64407-67-6
• Molecular Formula: C7H9ClN2O2
• Molecular Weight: 188.614
• Mol file: 64407-67-6.mol

Synonyms:Desamino (αS)-Chloro Histidine Methyl Ester;Desamino (aS)-Chloro Histidine Methyl Ester;Desamino (AlphaS)-Chloro Histidine Methyl Ester;

Chemical Property of Desamino (αS)-Chloro Histidine Methyl Ester

Chemical Property:

• PSA: 54.98000
• LogP: 0.73260

Purity/Quality:

97% ^*data from raw suppliers

Desamino(αS)-ChloroHistidineMethylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Histidine derivative.

Technology Process of Desamino (αS)-Chloro Histidine Methyl Ester

There total 1 articles about Desamino (αS)-Chloro Histidine Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methanol (67-56-1) + L-3-(1H-imidazol-4-yl)-2-chloropropionic acid (17561-26-1) → methyl 3-(imidazol-4(5)-yl)-2-chloropropanoate (64407-67-6)

Guidance literature:

With sulfuric acid; sodium sulfate; for 15h; Reflux;

DOI:10.3987/COM-09-S(S)127

Reference yield: 60.0%

methyl 3-(imidazol-4(5)-yl)-2-chloropropanoate (64407-67-6) → methyl 3-(imidazol-4(5)-yl)-2-propenoate (160073-02-9,52363-40-3)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 0 - 70 ℃;

DOI:10.3987/COM-09-S(S)127

upstream raw materials:

methanol

L-3-(1H-imidazol-4-yl)-2-chloropropionic acid

Downstream raw materials:

methyl 3-(imidazol-4⁽⁵⁾-yl)-2-propenoate

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