Benzoic acid, 3-hydroxy-2-pentyl-4,6-bis(phenylmethoxy)-, phenylmethyl ester

Base Information

• Chemical Name: Benzoic acid, 3-hydroxy-2-pentyl-4,6-bis(phenylmethoxy)-, phenylmethyl ester
• CAS No.: 64750-25-0
• Molecular Formula: C33H34O5
• Molecular Weight: 510.63

Synonyms:

Chemical Property of Benzoic acid, 3-hydroxy-2-pentyl-4,6-bis(phenylmethoxy)-, phenylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Benzoic acid, 3-hydroxy-2-pentyl-4,6-bis(phenylmethoxy)-, phenylmethyl ester

There total 12 articles about Benzoic acid, 3-hydroxy-2-pentyl-4,6-bis(phenylmethoxy)-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzyl 4,6-bis(benzyloxy)-3-formyl-2-pentylbenzoate (64750-24-9) → benzyl 4,6-bis(benzyloxy)-3-hydroxy-2-pentylbenzoate (64750-25-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 10 - 20 ℃; for 4h; Inert atmosphere;

Reference yield:

4,6-Bis-benzyloxy-3-formyloxy-2-pentyl-benzoic acid benzyl ester → benzyl 4,6-bis(benzyloxy)-3-hydroxy-2-pentylbenzoate (64750-25-0)

Guidance literature:

With potassium hydroxide; In methanol; at 0 ℃; for 0.75h; Yield given;

Reference yield:

C34H34O6 → benzyl 4,6-bis(benzyloxy)-3-hydroxy-2-pentylbenzoate (64750-25-0)

Guidance literature:

With potassium hydroxide; In methanol; water; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1021/acs.jnatprod.8b00227

upstream raw materials:

4-hydroxysalicylic acid

benzyl bromide

benzyl 2,4-bis(benzyloxy)benzoate

benzyl 4,6-bis(benzyloxy)-3-formyl-2-pentylbenzoate

Downstream raw materials:

lobaric acid

lobarin

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