Mesityloxide

Base Information

Chemical Name:Mesityloxide
CAS No.:64826-30-8
Molecular Formula:C18H22O
Molecular Weight:254.372
Hs Code.:
DSSTox Substance ID:DTXSID80494589
Wikidata:Q82342051

Synonyms:mesityloxide;64826-30-8;Benzene, 1,1'-oxybis[2,4,6-trimethyl-;1,3,5-TRIMETHYL-2-(2,4,6-TRIMETHYLPHENOXY)BENZENE;2,4,6-trimethylphenyl ether;SCHEMBL242786;DTXSID80494589;OZXIZRZFGJZWBF-UHFFFAOYSA-N;AKOS024437597;1,1'-Oxybis(2,4,6-trimethylbenzene)

Suppliers and Price of Mesityloxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Mesityloxide

Chemical Property:

XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:254.167065321
Heavy Atom Count:19
Complexity:235

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)OC2=C(C=C(C=C2C)C)C)C

Technology Process of Mesityloxide

There total 5 articles about Mesityloxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 4028-63-1
iodomesitylene

: 3360-56-3
1,3,5-trimethyl-2-trifluoromethylbenzene

: 64826-30-8
Dimesitylether

: 108-67-8
1,3,5-trimethyl-benzene

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; sodium 2,2,2-trifluoroacetate; at 150 - 180 ℃; for 15h;
DOI:10.1246/cl.1982.135

Reference yield: 35.0%

: 4028-63-1
iodomesitylene

: 2923-18-4
sodium 2,2,2-trifluoroacetate

: 3360-56-3
1,3,5-trimethyl-2-trifluoromethylbenzene

: 64826-30-8
Dimesitylether

: 108-67-8
1,3,5-trimethyl-benzene

Guidance literature:: With copper(l) iodide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 150 - 180 ℃; for 15h;
DOI:10.1246/cl.1982.135

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 64826-30-8
Dimesitylether

: tert-butyldimethyl(2,4,6-trimethylphenoxy)silane

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C

2.1: 0.5 h

3.1: sodium hexamethyldisilazane / toluene / 0.17 h / 0 - 25 °C / Inert atmosphere; Schlenk technique

3.2: 12 h / 0 - 25 °C / Schlenk technique; Inert atmosphere

With iodine; sodium hexamethyldisilazane; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1021/acs.orglett.8b00287