Rhodium(1+), tris(triphenylphosphine)-, perchlorate, compd. withdichloromethane (1:1)

Base Information

• Chemical Name: Rhodium(1+), tris(triphenylphosphine)-, perchlorate, compd. withdichloromethane (1:1)
• CAS No.: 64827-32-3
• Molecular Formula: C54H45P3Rh.CH2Cl2.ClO4
• Molecular Weight: 1074.16

Synonyms:Rhodium(1+), tris(triphenylphosphine)-, perchlorate, compd. withdichloromethane (1:1)

Chemical Property of Rhodium(1+), tris(triphenylphosphine)-, perchlorate, compd. withdichloromethane (1:1)

Chemical Property:

Purity/Quality:

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Technology Process of Rhodium(1+), tris(triphenylphosphine)-, perchlorate, compd. withdichloromethane (1:1)

There total 5 articles about Rhodium(1+), tris(triphenylphosphine)-, perchlorate, compd. withdichloromethane (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Wilkinson's catalyst (14694-95-2) → {Rh(P(C6H5)3)3}(1+)*ClO4(1-)*CH2Cl2={Rh(P(C6H5)3)3}ClO4*CH2Cl2 (64827-32-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: dichloromethane

In dichloromethane; acetone;

Reference yield:

{Rh(P(C6H5)3)3(OC(CH3)2)}(1+)*ClO4(1-)={Rh(P(C6H5)3)3(OC(CH3)2)}ClO4 (69880-15-5) + dichloromethane (75-09-2) → {Rh(P(C6H5)3)3}(1+)*ClO4(1-)*CH2Cl2={Rh(P(C6H5)3)3}ClO4*CH2Cl2 (64827-32-3)

Guidance literature:

In dichloromethane; by crystn. from oxygen-free CH2Cl2;

DOI:10.1021/ja00463a059

Reference yield:

{Rh(P(C6H5)3)3C2H5OH}(1+)*ClO4(1-)={Rh(P(C6H5)3)3(C2H5OH)}ClO4 + dichloromethane (75-09-2) → {Rh(P(C6H5)3)3}(1+)*ClO4(1-)*CH2Cl2={Rh(P(C6H5)3)3}ClO4*CH2Cl2 (64827-32-3)

Guidance literature:

In dichloromethane; by crystn. from oxygen-free CH2Cl2;

DOI:10.1021/ja00463a059

upstream raw materials:

{Rh(P(C₆H₅)3)3(OC(CH₃)2)}⁽¹⁺⁾*ClO₄^(1-)={Rh(P(C₆H₅)3)3(OC(CH₃)2)}ClO₄

dichloromethane

Wilkinson's catalyst

Rh(PPh₃)3⁽¹⁺⁾*BF₄^(1-)

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