Cyclohexyldodecylamine

Base Information

• Chemical Name: Cyclohexyldodecylamine
• CAS No.: 6490-87-5
• Molecular Formula: C18H37N
• Molecular Weight: 267.498
• Hs Code.: 2921300090
• Mol file: 6490-87-5.mol

Synonyms:Cyclohexyl-dodecylamin;cyclohexyl-dodecyl-amine;Cyclohexyl-dodecyl-amin;

Chemical Property of Cyclohexyldodecylamine

Chemical Property:

• PSA: 12.03000
• LogP: 6.22050

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexyldodecylamine

There total 18 articles about Cyclohexyldodecylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

n-Dodecylamine (124-22-1) + cyclohexanol (108-93-0) → N-dodecylcyclohexanamine (6490-87-5)

Guidance literature:

With NiCuFeO(x); In 5,5-dimethyl-1,3-cyclohexadiene; for 24h; Inert atmosphere; Sealed tube; Reflux;

DOI:10.1002/chem.201203417

Reference yield: 29.0%

N-cyclohexyl-N-dodecyl-p-toluenesulfonamide (84200-42-0) → N-dodecylcyclohexanamine (6490-87-5) + N-Cyclohexyl-N-dodecyl-formamide (84200-51-1)

Guidance literature:

With perhydrodibenzo-18-crown-6; In diethylene glycol dimethyl ether; for 3h; Ambient temperature;

DOI:10.1248/cpb.30.3178

Reference yield: 23.0%

N-cyclohexyl-N-dodecyl-mesylamide (84200-43-1) → N-dodecylcyclohexanamine (6490-87-5) + N-Cyclohexyl-N-dodecyl-formamide (84200-51-1)

Guidance literature:

With perhydrodibenzo-18-crown-6; In diethylene glycol dimethyl ether; for 3h; Ambient temperature;

DOI:10.1248/cpb.30.3178

upstream raw materials:

N-cyclohexyl-lauramide

n-Dodecylamine

cyclohexanone

1-Iodododecane

Downstream raw materials:

N-cyclohexyl,-N-dodecylacetamide

Refernces

• 1、 Ohsawa,Takagaki,Ikehara,et al.. "Reductive removal of sulfonyl groups: Cleavage of sulfonamides and sulfonates by alkali metal combined with crown ether". . p. 3178 - 3186. Retrieved 2007/10/02.