2,6-Piperidinedione,4-[2-[(1R,3S,5R)-3,5-dimethyl-2-oxocyclohexyl]-2-hydroxyethyl]-, rel-

Base Information

Chemical Name:2,6-Piperidinedione,4-[2-[(1R,3S,5R)-3,5-dimethyl-2-oxocyclohexyl]-2-hydroxyethyl]-, rel-
CAS No.:29106-61-4
Molecular Formula:C₁₅H₂₃NO₄
Molecular Weight:281.352
Hs Code.:

Synonyms:2,6-Piperidinedione,4-[2-(3,5-dimethyl-2-oxocyclohexyl)-2-hydroxyethyl]-; Neocycloheximide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-Piperidinedione,4-[2-[(1R,3S,5R)-3,5-dimethyl-2-oxocyclohexyl]-2-hydroxyethyl]-, rel-

Chemical Property:

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Technology Process of 2,6-Piperidinedione,4-[2-[(1R,3S,5R)-3,5-dimethyl-2-oxocyclohexyl]-2-hydroxyethyl]-, rel-

There total 7 articles about 2,6-Piperidinedione,4-[2-[(1R,3S,5R)-3,5-dimethyl-2-oxocyclohexyl]-2-hydroxyethyl]-, rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 3428-71-5,15676-38-7
C₁₆H₂₆N₄O₄

: 66-81-9,642-81-9,1154-57-0,3226-22-0,4630-75-5,5549-69-9,6258-25-9,6746-42-5,17280-60-3,17973-87-4,18006-33-2,29106-61-4,94130-62-8,94130-63-9,94799-82-3,95272-16-5,95272-17-6,95272-18-7
4-[(S)-2-((1S,3S,5S)-3,5-Dimethyl-2-oxo-cyclohexyl)-2-hydroxy-ethyl]-piperidine-2,6-dione

Guidance literature:: With acetic acid; sodium nitrite; In water; at 0 ℃; for 0.25h; pH=5;
DOI:10.1016/S0040-4020(01)91400-0

Reference yield:

: 2066-88-8
(2,6-dioxo-piperidin-4-yl)-acetaldehyde

: 93921-42-7
(+)-(2S,4R)-trans-2,4-dimethyl-1-cyclohexanone

: 94130-63-9
(2S,4S,6R,αS)-cycloheximide

: 66-81-9,642-81-9,1154-57-0,3226-22-0,4630-75-5,5549-69-9,6258-25-9,6746-42-5,17280-60-3,17973-87-4,18006-33-2,29106-61-4,94130-62-8,94130-63-9,94799-82-3,95272-16-5,95272-17-6,95272-18-7
(2S,4S,6S,αS)-cycloheximide

: 642-81-9
Cycloheximide

: 66-81-9
Cycloheximide

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -70 ℃; for 0.5h; Yield given. Yields of byproduct given;
DOI:10.1271/bbb1961.48.2315

Reference yield:

: 2066-88-8
(2,6-dioxo-piperidin-4-yl)-acetaldehyde

: ((4R,6S)-4,6-Dimethyl-cyclohex-1-enyloxy)-trimethyl-silane

: 94130-63-9
(2S,4S,6R,αS)-cycloheximide

: 66-81-9,642-81-9,1154-57-0,3226-22-0,4630-75-5,5549-69-9,6258-25-9,6746-42-5,17280-60-3,17973-87-4,18006-33-2,29106-61-4,94130-62-8,94130-63-9,94799-82-3,95272-16-5,95272-17-6,95272-18-7
(2S,4S,6S,αS)-cycloheximide

: 642-81-9
Cycloheximide

: 66-81-9
Cycloheximide

Guidance literature:: With titanium tetrachloride; In dichloromethane; Yield given. Yields of byproduct given; 1.) 20 deg C, 5 min, 2.) -45 deg C, 5 min;
DOI:10.1271/bbb1961.48.2315