1-(4-methoxyphenyl)ethanone [1-(4-methoxyphenyl)ethylidene]hydrazone

Base Information

• Chemical Name: 1-(4-methoxyphenyl)ethanone [1-(4-methoxyphenyl)ethylidene]hydrazone
• CAS No.: 65124-88-1
• Molecular Formula: C18H20N2O2
• Molecular Weight: 296.369
• Mol file: 65124-88-1.mol

Synonyms:4,4'-dimethoxyacetophenone azine;4,4'-dimethoxy-α,α'-dimethylbenzalazine;

Chemical Property of 1-(4-methoxyphenyl)ethanone [1-(4-methoxyphenyl)ethylidene]hydrazone

Chemical Property:

• PSA: 43.18000
• LogP: 3.93700

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4-methoxyphenyl)ethanone [1-(4-methoxyphenyl)ethylidene]hydrazone

There total 11 articles about 1-(4-methoxyphenyl)ethanone [1-(4-methoxyphenyl)ethylidene]hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-methoxyacetophenone hydrazone (6310-14-1) → 1-(4-methoxyphenyl)ethanone <1-(4-methoxyphenyl)ethylidene>hydrazone (65124-88-1)

Guidance literature:

With oxygen; In methanol; for 1h; Ambient temperature;

DOI:10.1016/S0040-4039(00)84608-0

Reference yield: 84.0%

1-(4-methoxyphenyl)ethanone (100-06-1) → 1-(4-methoxyphenyl)ethanone <1-(4-methoxyphenyl)ethylidene>hydrazone (65124-88-1)

Guidance literature:

With hydrazine hydrate; acetic acid; In ethanol; for 10h; Reflux;

DOI:10.1021/ol501483k

Reference yield: 22.0%

4-(4-methoxyphenyl)-2-methyl-6-oxo-2H-pyran-3-carboxylic acid (67075-05-2) → 1-(4-methoxyphenyl)ethanone <1-(4-methoxyphenyl)ethylidene>hydrazone (65124-88-1)

Guidance literature:

With hydrazine hydrate; In ethanol; for 2h; Heating;

upstream raw materials:

4-methoxyacetophenone hydrazone

4-(4-methoxyphenyl)-2-methyl-6-oxo-2H-pyran-3-carboxylic acid

isopropyl alcohol

tert-butyl alcohol

Downstream raw materials:

3-(4-methoxyphenyl)-1-[1-(4-methoxyphenyl)vinyl]-1H-4-pyrazolecarbaldehyde