Ethanone, 1-(2-bromo-5-nitrophenyl)-

Base Information

• Chemical Name: Ethanone, 1-(2-bromo-5-nitrophenyl)-
• CAS No.: 65130-31-6
• Molecular Formula: C8H6BrNO3
• Molecular Weight: 244.045

Synonyms:2-bromo-5-nitroacetophenone;6-Brom-3-nitro-acetophenon;1-(2-bromo-5-nitro-phenyl)-ethanone;2-Brom-5-nitro-acetophenon;1-(2-Brom-5-nitro-phenyl)-aethanon;

Chemical Property of Ethanone, 1-(2-bromo-5-nitrophenyl)-

Chemical Property:

• PSA: 62.89000
• LogP: 3.08310

Purity/Quality:

99% ^*data from raw suppliers

1-(2-BROMO-5-NITROPHENYL)ETHANONE 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Ethanone, 1-(2-bromo-5-nitrophenyl)-

There total 7 articles about Ethanone, 1-(2-bromo-5-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

2-bromophenyl methyl ketone (2142-69-0) → 1-(2′-bromo-5′-nitrophenyl)ethan-1-one (65130-31-6) + 1-(2-bromo-3-nitro-phenyl)ethanone (135007-62-4)

Guidance literature:

With sulfuric acid; potassium nitrate; In water; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1002/chem.202003209

Reference yield: 55.0%

α-bromoacetophenone (70-11-1) → 1-(2′-bromo-5′-nitrophenyl)ethan-1-one (65130-31-6)

Guidance literature:

With potassium nitrate; In sulfuric acid; water; at 0 - 20 ℃; for 1.16667h;

DOI:10.1002/chem.201304241

Reference yield: 54.0%

2-bromophenyl methyl ketone (2142-69-0) → 1-(2′-bromo-5′-nitrophenyl)ethan-1-one (65130-31-6)

Guidance literature:

With sulfuric acid; potassium nitrate; at 0 - 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1021/acs.joc.7b02287

upstream raw materials:

2-bromophenyl methyl ketone

1-(2-amino-5-nitro-phenyl)ethanone

2-bromo-5-nitrobenzoyl chloride

2-aminoacetophenone

Downstream raw materials:

1-[2-(2-amino-phenylsulfanyl)-5-nitro-phenyl]-ethanone

(S)-1-(2-Bromo-5-nitro-phenyl)-ethanol

1-[(R)-1-(2-Bromo-5-nitro-phenyl)-ethyl]-pyrrolidine

α-6-bromo-3-nitro-acetophenone oxime

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