Benzofuran, 2-(3,5-dimethoxyphenyl)-

Base Information

Chemical Name:Benzofuran, 2-(3,5-dimethoxyphenyl)-
CAS No.:65246-42-6
Molecular Formula:C16H14O3
Molecular Weight:254.285
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzofuran, 2-(3,5-dimethoxyphenyl)-

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Technology Process of Benzofuran, 2-(3,5-dimethoxyphenyl)-

There total 15 articles about Benzofuran, 2-(3,5-dimethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 98437-24-2
benzofuran-2-boronic acid

: 20469-65-2
1-bromo-3,5-dimethoxybenzene

: 65246-42-6
2-(3,5-dimethoxyphenyl)benzofuran

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 90 ℃; for 8h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201502595

Reference yield: 79.0%

: 533-58-4
2-Iodophenol

: 171290-52-1
1-Ethynyl-3,5-dimethoxy-benzene

: 65246-42-6
2-(3,5-dimethoxyphenyl)benzofuran

Guidance literature:: With dichloro{2-[(1H-pyrazol-1-yl-κN²)methyl]-6-(1H-pyrazol-1-yl-κN²)pyridine-κN}copper(II); caesium carbonate; In 1,4-dioxane; at 130 ℃; for 48h; Sealed tube; Inert atmosphere;
DOI:10.1002/adsc.201301010

Reference yield: 71.0%

: 18698-97-0
ortho-bromophenylacetic acid

: 2150-37-0
methyl 3,5-dimethoxybenzoate

: 65246-42-6
2-(3,5-dimethoxyphenyl)benzofuran

Guidance literature:: ortho-bromophenylacetic acid; methyl 3,5-dimethoxybenzoate; With sodium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; at -10 ℃; for 3.5h; Inert atmosphere;

With potassium dihydrogenphosphate; copper(l) iodide; potassium phosphate tribasic heptahydrate; In tetrahydrofuran; N,N-dimethyl-formamide; at 110 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c2gc16457d