Technology Process of 3-(hexadecyloxy)-2-methoxypropyl 2-(pyridinium-1-yl)ethyl phosphate
There total 4 articles about 3-(hexadecyloxy)-2-methoxypropyl 2-(pyridinium-1-yl)ethyl phosphate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / benzene / 2 h / O deg C to room temp.
2: H2O / 1.5 h / Heating
3: 2.) Ag2CO3 / 1.) 1.5 h reflux, 2.) methanol, 1 h reflux
With
pyridine; silver carbonate;
In
water; benzene;
DOI:10.1248/cpb.30.3260
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2O / 1.5 h / Heating
2: 2.) Ag2CO3 / 1.) 1.5 h reflux, 2.) methanol, 1 h reflux
With
silver carbonate;
In
water;
DOI:10.1248/cpb.30.3260
- Guidance literature:
-
Multi-step reaction with 4 steps
1: KOH / tetrahydrofuran; dimethylsulfoxide / 2 h / Ambient temperature
2: pyridine / benzene / 2 h / O deg C to room temp.
3: H2O / 1.5 h / Heating
4: 2.) Ag2CO3 / 1.) 1.5 h reflux, 2.) methanol, 1 h reflux
With
pyridine; potassium hydroxide; silver carbonate;
In
tetrahydrofuran; water; dimethyl sulfoxide; benzene;
DOI:10.1248/cpb.30.3260
