9H-Thioxanthen-9-one,monohydriodide

Base Information

Chemical Name:9H-Thioxanthen-9-one,monohydriodide
CAS No.:80568-29-2
Molecular Formula:C₁₈H₂₀N₂O₂S*HI
Molecular Weight:456.347
Hs Code.:
ChEMBL ID:CHEMBL1968826
DSSTox Substance ID:DTXSID70542482
NSC Number:317003

Synonyms:NSC317003;80568-29-2;9H-Thioxanthen-9-one,monohydriodide;CHEMBL1968826;DTXSID70542482;NSC-317003;1-{[2-(Dimethylamino)ethyl]amino}-7-hydroxy-4-methyl-9H-thioxanthen-9-one--hydrogen iodide (1/1)

Suppliers and Price of 9H-Thioxanthen-9-one,monohydriodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 9H-Thioxanthen-9-one,monohydriodide

Chemical Property:

Vapor Pressure:3.97E-12mmHg at 25°C
Boiling Point:536.6°Cat760mmHg
Flash Point:278.3°C
Density:1.298g/cm³
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:456.03685
Heavy Atom Count:24
Complexity:431

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C(=C(C=C1)NCCN(C)C)C(=O)C3=C(S2)C=CC(=C3)O.I

Technology Process of 9H-Thioxanthen-9-one,monohydriodide

There total 8 articles about 9H-Thioxanthen-9-one,monohydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6705-03-9
2-Amino-5-methoxybenzoic acid

: 80568-29-2
1-<<2-(dimethylamino)ethyl>amino>-7-hydroxy-4-methylthixanthenone

Guidance literature:: Multi-step reaction with 3 steps

1: conc. H₂SO₄

2: pyridine / 20 h / Heating

3: 1.7 g / 48percent HI / 3 h / Heating

With pyridine; sulfuric acid; hydrogen iodide;
DOI:10.1021/jm00345a006

Reference yield:

: 27139-97-5
2-bromo-4-chloro-1-methyl-benzene

: 80568-29-2
1-<<2-(dimethylamino)ethyl>amino>-7-hydroxy-4-methylthixanthenone

Guidance literature:: Multi-step reaction with 4 steps

1: 18.5 g / K₂CO₃, KI, Cu bronze / dimethylformamide / 18 h / Heating

2: 200 mg / conc. H₂SO₄ / 1.5 h / Heating

3: pyridine / 20 h / Heating

4: 1.7 g / 48percent HI / 3 h / Heating

With pyridine; copper bronze; sulfuric acid; hydrogen iodide; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00345a006

Reference yield:

: 16807-37-7
5-methoxy-2-sulfanyl-benzoic acid

: 80568-29-2
1-<<2-(dimethylamino)ethyl>amino>-7-hydroxy-4-methylthixanthenone

Guidance literature:: Multi-step reaction with 4 steps

1: 18.5 g / K₂CO₃, KI, Cu bronze / dimethylformamide / 18 h / Heating

2: 200 mg / conc. H₂SO₄ / 1.5 h / Heating

3: pyridine / 20 h / Heating

4: 1.7 g / 48percent HI / 3 h / Heating

With pyridine; copper bronze; sulfuric acid; hydrogen iodide; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00345a006