Propanenitrile, 3,3'-(1,2-ethanediyldiimino)bis-

Base Information

• Chemical Name: Propanenitrile, 3,3'-(1,2-ethanediyldiimino)bis-
• CAS No.: 3217-00-3
• Molecular Formula: C8H14 N4
• Molecular Weight: 166.226
• Hs Code.: 2926909090
• European Community (EC) Number: 221-738-1
• NSC Number: 4412
• UNII: VL6H50RQF4
• DSSTox Substance ID: DTXSID1062910
• Nikkaji Number: J262.323D
• Wikidata: Q81990349
• Mol file: 3217-00-3.mol

Synonyms:3217-00-3;Propanenitrile, 3,3'-(1,2-ethanediyldiimino)bis-;4,7-Diazadecane-1,10-dinitrile;N,N'-Bis(2-cyanoethyl)ethylenediamine;3,3'-(Ethylenediimino)bispropiononitrile;3-[2-(2-cyanoethylamino)ethylamino]propanenitrile;1,2-Bis(2-cyanoethylamino)ethane;3-[2-(2-Cyano-ethylamino)-ethylamino]-propionitrile;3,3-(ethylenediimino)bispropiononitrile;VL6H50RQF4;3-({2-[(2-cyanoethyl)amino]ethyl}amino)propanenitrile;Propionitrile, 3,3'-(ethylenediimino)di-;NSC 4412;NSC-4412;EINECS 221-738-1;N,N'-(beta-Cyanoethyl)ethylenediamine;N,N'-(.beta.-Cyanoethyl)ethylenediamine;N,N-Bis-(beta-cyanoethyl)ethylene diamine;N,N'-Bis(2-cyanoethyl)-1,2-ethanediamine;N,N'-Di(2-cyanoethyl)-1,2-ethylenediamine;EC 221-738-1;NSC4412;4,10-dinitrile;UNII-VL6H50RQF4;SCHEMBL1188228;DTXSID1062910;AKOS000115520;Propionitrile,3'-(ethylenediimino)di-;CS-0218873;N,N-Bis-(.beta.-cyanoethyl)ethylene diamine;EN300-02347;Propanenitrile,3'-(1,2-ethanediyldiimino)bis-;N,N-BIS(.BETA.-CYANOETHYL)ETHYLENEDIAMINE;W-109878;3,3'-(1,2-ETHANEDIYLDIIMINO)BIS(PROPANENITRILE)

Chemical Property of Propanenitrile, 3,3'-(1,2-ethanediyldiimino)bis-

Chemical Property:

• Boiling Point: 383.2°Cat760mmHg
• Flash Point: 185.5°C
• PSA: 71.64000
• Density: 1.007g/cm³
• LogP: 0.77476
• XLogP3: -1.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 166.121846464
• Heavy Atom Count: 12
• Complexity: 160

Purity/Quality:

99.9% ^*data from raw suppliers

3-[2-(2-CYANO-ETHYLAMINO)-ETHYLAMINO]-PROPIONITRILE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CNCCNCCC#N)C#N

Technology Process of Propanenitrile, 3,3'-(1,2-ethanediyldiimino)bis-

There total 5 articles about Propanenitrile, 3,3'-(1,2-ethanediyldiimino)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.98%

ethylenediamine (107-15-3,85404-18-8) + acrylonitrile (107-13-1,25014-41-9) → N,N'-bis-(2-cyanoethyl)ethylenediamine (3217-00-3)

Guidance literature:

at 20 - 25 ℃; for 26h; Temperature;

Reference yield:

ethylenediamine (107-15-3,85404-18-8) + acrylonitrile (107-13-1,25014-41-9) → N,N'-bis-(2-cyanoethyl)ethylenediamine (3217-00-3) + N,N,N′,N′-tetrakis(2-cyanoethyl)-1,2-ethylenediamine (45243-86-5) + N,N,N'-tris(2-cyanoethyl)-1,2-ethylenediamine (56576-72-8) + N-(β-cyanoethyl)ethylenediamine (22584-31-2,25609-52-3)

Guidance literature:

In water; at 60 ℃; for 6.5h;

Reference yield:

ethylenediamine (107-15-3,85404-18-8) + acrylonitrile (107-13-1,25014-41-9) → N,N'-bis-(2-cyanoethyl)ethylenediamine (3217-00-3) + N,N,N'-tris(2-cyanoethyl)-1,2-ethylenediamine (56576-72-8) + N-(β-cyanoethyl)ethylenediamine (22584-31-2,25609-52-3)

Guidance literature:

at 50 - 70 ℃; for 2 - 4.5h; Product distribution / selectivity;

upstream raw materials:

ethylenediamine

acrylonitrile

Downstream raw materials:

N,N,N'-tris(3-aminopropyl)ethylenediamine

N-(2-Aminoethyl)-1,3-propanediamine

N,N'-bis(3-aminopropyl)-1,2-diamine

triethylentetramine

Refernces

• 1、 Ivanova,I.S. et al.. "-". . . Retrieved 1962.
• 2、 -. "METHOD FOR PREPARING N,N'-BIS(2-CYANOETHYL)-1,2-ETHYLENEDIAMINE". Paragraph 0027-0030; 0056. . Retrieved 2017/06/21.
• 3、 -. "PREPARATION METHOD OF HIGH SELECTIVITY N, N'-BIS(2-CYANOETHYL)-1,2-ETHYLENEDIAMINE". Paragraph 0023; 0025; 0027; 0028; 0029; 0031; 0033; 0038. . Retrieved 2017/09/12.