7-METHYL-2,3-DIHYDROISOINDOLE-1-ONE

Base Information

• Chemical Name: 7-METHYL-2,3-DIHYDROISOINDOLE-1-ONE
• CAS No.: 65399-02-2
• Molecular Formula: C9H9NO
• Molecular Weight: 147.17400
• Hs Code.: 2933790090

Synonyms:7-Methylisoindolin-1-on;7-methylisoindolin-1-one;7-Methylisoindolinone;7-methyl-2,3-dihydro-isoindol-1-one;7-METHYL-2,3-DIHYDROISOINDOLE-1-ONE;

Chemical Property of 7-METHYL-2,3-DIHYDROISOINDOLE-1-ONE

Chemical Property:

• Boiling Point: 394.5±42.0 °C(Predicted)
• PKA: 14.44±0.20(Predicted)
• PSA: 32.59000
• Density: 1.155±0.06 g/cm3(Predicted)
• LogP: 1.24880
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

7-Methylisoindolin-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-METHYL-2,3-DIHYDROISOINDOLE-1-ONE

There total 14 articles about 7-METHYL-2,3-DIHYDROISOINDOLE-1-ONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

D2916 (130403-08-6) → 7-methyl-3H-isobenzofuran-1-one (2211-84-9) + 7-Methyl-2,3-dihydroisoindole-1-one (65399-02-2) + N-(5-Methylisoxazol-3-yl)-7-methylisoindolinone

Guidance literature:

With sodium persulfate; copper diacetate; sodium acetate; acetic acid; for 8h; Heating;

DOI:10.1016/S0014-827X(98)00057-3

Reference yield: 14.0%

N-(5-Methylisoxazol-3-yl)-7-methylisoindolinone → 7-Methyl-2,3-dihydroisoindole-1-one (65399-02-2)

Guidance literature:

With sodium persulfate; copper diacetate; sodium acetate; acetic acid; for 8h; Heating;

DOI:10.1016/S0014-827X(98)00057-3

Reference yield: 12.0%

2,6-dimethylbenzamide (55321-98-7) → 7-Methyl-2,3-dihydroisoindole-1-one (65399-02-2)

Guidance literature:

With sodium persulfate; copper diacetate; sodium acetate; acetic acid; for 8h; Heating;

DOI:10.1016/S0014-827X(98)00057-3

upstream raw materials:

<(2-Azidomethyl-6-methylbenzoyl)(methyl)amino>methyl-2-(<(tert-butoxy)carbonyl>amino)-3-phenylpropanoate

2,6-dimethylbenzamide

D₂₉₁₆

2,6-dimethylbenzoyl chloride

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