6-chloro-3-methyl-4H-1,2,4-benzothiadiazine-7-sulfonamide 1,1-dioxide

Base Information

Chemical Name:6-chloro-3-methyl-4H-1,2,4-benzothiadiazine-7-sulfonamide 1,1-dioxide
CAS No.:1025-75-8
Molecular Formula:C8H8 Cl N3 O4 S2
Molecular Weight:309.7498
Hs Code.:

Synonyms:6-chloro-3-methyl-1,1-dioxo-4H-1;6-chloro-3-methyl-4h-1,2,4-benzothiadiazine-7-sulfonamide 1,1-dioxide;2H-1,2,4-Benzothiadiazine-7-sulfonamide,6-chloro-3-methyl-,1,1-dioxide;6-Chlor-3-methyl-1,2,4-benzothiadiazin-7-sulfonamid-1,1-dioxid;6-Chlor-3-methyl-7-sulfamoyl-1,2,4-benzothiadiazin-1,1-dioxid;6-Chloro-3-methyl-2H-1,2,4-benzothiadiazine-7-sulfonamide 1,1-dioxide;3-Methyl-6-chlor-1.2.4-benzothiadiazin-7-sulfonamid-1.1-dioxid;

Suppliers and Price of 6-chloro-3-methyl-4H-1,2,4-benzothiadiazine-7-sulfonamide 1,1-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 6-chloro-3-methyl-4H-1,2,4-benzothiadiazine-7-sulfonamide 1,1-dioxide

Chemical Property:

Vapor Pressure:4.29E-14mmHg at 25°C
Boiling Point:594.3°Cat760mmHg
Flash Point:313.2°C
PSA：135.45000
Density:1.93g/cm³
LogP:2.95550

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-chloro-3-methyl-4H-1,2,4-benzothiadiazine-7-sulfonamide 1,1-dioxide

There total 7 articles about 6-chloro-3-methyl-4H-1,2,4-benzothiadiazine-7-sulfonamide 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100191-64-8
4-acetylamino-6-chloro-benzene-1,3-disulfonyl chloride

: 1025-75-8
IDRA 22

Guidance literature:: With ammonia; anschliessend Erhitzen auf 200grad;
DOI:10.1021/ja01565a079

Reference yield:

: 121-30-2
chloraminophenamide

: 75-07-0,9002-91-9
acetaldehyde

: 1025-75-8
6-chloro-3-methyl-1,1-dioxo-1,2(4)-dihydro-1λ⁶-benzo[1,2,4]thiadiazine-7-sulfonic acid amide

Guidance literature:: chloraminophenamide; acetaldehyde; In N,N-dimethyl-formamide; Reflux;

With potassium permanganate; sodium hydroxide;
DOI:10.1139/cjc-2019-0194

Reference yield:

: 121-30-2
chloraminophenamide

: 1025-75-8
6-chloro-3-methyl-1,1-dioxo-1,2(4)-dihydro-1λ⁶-benzo[1,2,4]thiadiazine-7-sulfonic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / Reflux

2: water / Heating; Alkaline conditions

In tetrahydrofuran; water;
DOI:10.1139/cjc-2019-0194