russuphelin A

Base Information

Chemical Name:russuphelin A
CAS No.:141794-49-2
Molecular Formula:C20H14 Cl4 O6
Molecular Weight:492.137
Hs Code.:
Mol file:141794-49-2.mol

Synonyms:RussuphelinA

Suppliers and Price of russuphelin A

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
RUSSUPHELIN A 95.00%
5MG
$ 495.64

Total 1 raw suppliers

Chemical Property of russuphelin A

Chemical Property:

Vapor Pressure:1.04E-12mmHg at 25°C
Boiling Point:550.1°Cat760mmHg
Flash Point:286.5°C
PSA：77.38000
Density:1.522g/cm³
LogP:7.31320

Purity/Quality:: RUSSUPHELIN A 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of russuphelin A

There total 13 articles about russuphelin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 186805-86-7
bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene

: 141794-49-2
4,4′-[(2,5-dimethoxy-1,3-phenylene)bis(oxy)]bis[3,5-dichlorophenol]

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 8h;
DOI:10.1080/00397919708004811

Reference yield:

: 20103-10-0
2,6-dichloro-1,4-benzenediol

: 141794-49-2
4,4′-[(2,5-dimethoxy-1,3-phenylene)bis(oxy)]bis[3,5-dichlorophenol]

Guidance literature:: Multi-step reaction with 8 steps

1: 66 percent / K₂CO₃ / acetone / 12 h / Ambient temperature

2: 92 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

3: 85 percent / H₂ / PtO₂ / ethyl acetate / 5 h / Ambient temperature

4: 66 percent / NaH / dimethylformamide / 3 h / Ambient temperature

5: NaH / dimethylformamide / 3 h / Ambient temperature

6: satd. aq. Na₂S₂O₄

7: 88 percent / K₂CO₃ / acetone / 6 h / 45 °C

8: 72 percent / CF₃COOH / CH₂Cl₂ / 8 h

With sodium dithionite; hydrogen; sodium hydride; potassium carbonate; trifluoroacetic acid; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1080/00397919708004811

Reference yield:

: 697-91-6
2,6-dichloro-1,4-benzoquinone

: 141794-49-2
4,4′-[(2,5-dimethoxy-1,3-phenylene)bis(oxy)]bis[3,5-dichlorophenol]

Guidance literature:: Multi-step reaction with 9 steps

1: 98 percent / satd. aq. Na₂S₂O₄ / CHCl₃

2: 66 percent / K₂CO₃ / acetone / 12 h / Ambient temperature

3: 92 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

4: 85 percent / H₂ / PtO₂ / ethyl acetate / 5 h / Ambient temperature

5: 66 percent / NaH / dimethylformamide / 3 h / Ambient temperature

6: NaH / dimethylformamide / 3 h / Ambient temperature

7: satd. aq. Na₂S₂O₄

8: 88 percent / K₂CO₃ / acetone / 6 h / 45 °C

9: 72 percent / CF₃COOH / CH₂Cl₂ / 8 h

With sodium dithionite; hydrogen; sodium hydride; potassium carbonate; trifluoroacetic acid; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1080/00397919708004811