bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene

Base Information

Chemical Name:bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene
CAS No.:186805-86-7
Molecular Formula:C₂₈H₃₀Cl₄O₁₀
Molecular Weight:668.352
Hs Code.:

Synonyms:bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene

Suppliers and Price of bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene

There total 7 articles about bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 77-78-1
dimethyl sulfate

: 186805-85-6
2,6-Bis-[2,6-dichloro-4-(2-methoxy-ethoxymethoxy)-phenoxy]-benzene-1,4-diol

: 186805-86-7
bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene

Guidance literature:: With potassium carbonate; In acetone; at 45 ℃; for 6h;
DOI:10.1080/00397919708004811

Reference yield:

: 20103-10-0
2,6-dichloro-1,4-benzenediol

: 186805-86-7
bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene

Guidance literature:: Multi-step reaction with 7 steps

1: 66 percent / K₂CO₃ / acetone / 12 h / Ambient temperature

2: 92 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

3: 85 percent / H₂ / PtO₂ / ethyl acetate / 5 h / Ambient temperature

4: 66 percent / NaH / dimethylformamide / 3 h / Ambient temperature

5: NaH / dimethylformamide / 3 h / Ambient temperature

6: satd. aq. Na₂S₂O₄

7: 88 percent / K₂CO₃ / acetone / 6 h / 45 °C

With sodium dithionite; hydrogen; sodium hydride; potassium carbonate; platinum(IV) oxide; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1080/00397919708004811

Reference yield:

: 697-91-6
2,6-dichloro-1,4-benzoquinone

: 186805-86-7
bis 2,6-[(2',6'-dichloro-4'-methoxy ethoxy methoxy)phenoxy]-1,4-dimethoxybenzene

Guidance literature:: Multi-step reaction with 8 steps

1: 98 percent / satd. aq. Na₂S₂O₄ / CHCl₃

2: 66 percent / K₂CO₃ / acetone / 12 h / Ambient temperature

3: 92 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

4: 85 percent / H₂ / PtO₂ / ethyl acetate / 5 h / Ambient temperature

5: 66 percent / NaH / dimethylformamide / 3 h / Ambient temperature

6: NaH / dimethylformamide / 3 h / Ambient temperature

7: satd. aq. Na₂S₂O₄

8: 88 percent / K₂CO₃ / acetone / 6 h / 45 °C

With sodium dithionite; hydrogen; sodium hydride; potassium carbonate; platinum(IV) oxide; In tetrahydrofuran; chloroform; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1080/00397919708004811