2-Furancarbonyl chloride, 5-(trifluoromethyl)- (9CI)

Base Information

Chemical Name:2-Furancarbonyl chloride, 5-(trifluoromethyl)- (9CI)
CAS No.:65865-25-0
Molecular Formula:C6H2ClF3O2
Molecular Weight:198.52700
Hs Code.:2932190090
Mol file:65865-25-0.mol

Synonyms:2-FURANCARBONYL CHLORIDE,5-(TRIFLUOROMETHYL);5-Trifluormethyl-furan-2-carbonsaeurechlorid;5-trifluoromethyl-furan-2-carbonyl chloride;

Suppliers and Price of 2-Furancarbonyl chloride, 5-(trifluoromethyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Furancarbonyl chloride, 5-(trifluoromethyl)- (9CI)

Chemical Property:

PSA：30.21000
LogP:2.67740

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Furancarbonyl chloride, 5-(trifluoromethyl)- (9CI)

There total 3 articles about 2-Furancarbonyl chloride, 5-(trifluoromethyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 56286-73-8
5-(trifluoromethyl)furan-2-carboxylic acid

: 65865-25-0
5-(trifluoromethyl)furan-2-carbonyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 ℃;
DOI:10.1016/j.bmcl.2012.10.034

Reference yield:

: 65865-28-3
(5-(trifluoromethyl)furan-2-yl)methanol

: 65865-25-0
5-(trifluoromethyl)furan-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chlorite; 2-methyl-but-2-ene; Dess-Martin periodane / dichloromethane; tert-butyl alcohol; aq. phosphate buffer / pH 7

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C

With sodium chlorite; 2-methyl-but-2-ene; oxalyl dichloride; Dess-Martin periodane; N,N-dimethyl-formamide; In aq. phosphate buffer; dichloromethane; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2012.10.034