Technology Process of 1H-Inden-1-one,
6,7-dichloro-2,3-dihydro-5-hydroxy-2-(4-methoxyphenyl)-2-methyl-
There total 9 articles about 1H-Inden-1-one,
6,7-dichloro-2,3-dihydro-5-hydroxy-2-(4-methoxyphenyl)-2-methyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
palladium;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: bromine; sodium hydrogensulfite / acetic acid
2: lithium bromide / N,N-dimethyl-formamide
3: (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid
4: pyridine hydrochloride
5: potassium carbonate / N-methyl-acetamide
6: potassium tert-butylate / water; tert-butyl alcohol
7: palladium / ethanol
With
lithium bromide; potassium tert-butylate; bromine; pyridine hydrochloride; potassium carbonate; sodium hydrogensulfite;
palladium;
In
N-methyl-acetamide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; ethanol; sulfuric acid; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine hydrochloride
2: potassium carbonate / N-methyl-acetamide
3: potassium tert-butylate / water; tert-butyl alcohol
4: palladium / ethanol
With
potassium tert-butylate; pyridine hydrochloride; potassium carbonate;
palladium;
In
N-methyl-acetamide; ethanol; water; tert-butyl alcohol;
