8-Decenamide, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N-[(3S)-4-[[(1,1-dimethylethyl)di methylsilyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]butyl]-2-methyl-, (8E)-

Base Information

Chemical Name:8-Decenamide, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N-[(3S)-4-[[(1,1-dimethylethyl)di methylsilyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]butyl]-2-methyl-, (8E)-
CAS No.:661462-00-6
Molecular Formula:C43H75NO4Si3
Molecular Weight:754.329
Hs Code.:

8-Decenamide,
3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N-[(3S)-4-[[(1,1-dimethylethyl)di
methylsilyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]butyl]-2-methyl-,
(8E)-

Synonyms:

Suppliers and Price of 8-Decenamide, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N-[(3S)-4-[[(1,1-dimethylethyl)di methylsilyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]butyl]-2-methyl-, (8E)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-Decenamide, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N-[(3S)-4-[[(1,1-dimethylethyl)di methylsilyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]butyl]-2-methyl-, (8E)-

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 8-Decenamide, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N-[(3S)-4-[[(1,1-dimethylethyl)di methylsilyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]butyl]-2-methyl-, (8E)-

There total 8 articles about 8-Decenamide, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N-[(3S)-4-[[(1,1-dimethylethyl)di methylsilyl]oxy]-3-[[(1,1-dimethylethyl)diphenylsilyl]oxy]butyl]-2-methyl-, (8E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 661462-07-3
(S)-4-azido-1-tert-butyldimethylsilyloxybutan-2-ol

: 661462-00-6
(E)-N-[(S)-4-tert-butyldimethylsilyloxy-3-tert-butyldiphenylsilyloxybutyl]-3-tert-butyldimethylsilyloxy-2-methyldec-8-enamide

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / imidazole; N,N-dimethylaminopyridine / dimethylformamide / 10 h / 20 °C

2: 100 percent / H₂ / 10 percent Pd-C / ethyl acetate / 3 h / 20 °C

3: 3.21 g / triethylamine / CH₂Cl₂ / 3 h / 20 °C

With 1H-imidazole; dmap; hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.3987/com-03-s64

Reference yield:

: 661461-98-9
(S)-4-azido-1-tert-butyldimethylsilyloxy-2-tert-butyldiphenylsilyloxybutane

: 661462-00-6
(E)-N-[(S)-4-tert-butyldimethylsilyloxy-3-tert-butyldiphenylsilyloxybutyl]-3-tert-butyldimethylsilyloxy-2-methyldec-8-enamide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 10 percent Pd-C / ethyl acetate / 3 h / 20 °C

2: 3.21 g / triethylamine / CH₂Cl₂ / 3 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.3987/com-03-s64