3-Cyclohexyl-2-hydroxybenzaldehyde

Base Information

Chemical Name:3-Cyclohexyl-2-hydroxybenzaldehyde
CAS No.:66232-33-5
Molecular Formula:C13H16O2
Molecular Weight:204.269
Hs Code.:
DSSTox Substance ID:DTXSID40503409
Nikkaji Number:J959.177J
Wikidata:Q82357199

Synonyms:3-Cyclohexyl-2-hydroxybenzaldehyde;3-Cyclohexylsalicylaldehyde;66232-33-5;2-hydroxy-3-cyclohexylbenzaldehyde;SCHEMBL1527151;DTXSID40503409;BHCSMURKCUUBKT-UHFFFAOYSA-N;MFCD24714445

Suppliers and Price of 3-Cyclohexyl-2-hydroxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Cyclohexyl-2-hydroxybenzaldehyde

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:204.115029749
Heavy Atom Count:15
Complexity:209

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)C2=CC=CC(=C2O)C=O

Technology Process of 3-Cyclohexyl-2-hydroxybenzaldehyde

There total 4 articles about 3-Cyclohexyl-2-hydroxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 119-42-6
2-cyclohexylphenol

: 66232-33-5
3-cyclohexyl-2-hydroxybenzaldehyde

Guidance literature:: 2-cyclohexylphenol; With triethylamine; magnesium chloride; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere;

formaldehyd; In tetrahydrofuran; for 3h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201210198

Reference yield:

: 108-85-0
1-bromocyclohexane

: 66232-33-5
3-cyclohexyl-2-hydroxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 h / 115 °C / Inert atmosphere

2.1: triethylamine; magnesium chloride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

2.2: 3 h / Inert atmosphere; Reflux

With triethylamine; magnesium chloride; In tetrahydrofuran;
DOI:10.1002/anie.201210198

Reference yield:

: 108-95-2,27073-41-2
phenol

: 66232-33-5
3-cyclohexyl-2-hydroxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 h / 115 °C / Inert atmosphere

2.1: triethylamine; magnesium chloride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

2.2: 3 h / Inert atmosphere; Reflux

With triethylamine; magnesium chloride; In tetrahydrofuran;
DOI:10.1002/anie.201210198