1-[2-(Diphenylmethoxy)ethyl]guanidine

Base Information

• Chemical Name: 1-[2-(Diphenylmethoxy)ethyl]guanidine
• CAS No.: 16136-32-6
• Molecular Formula: C₁₆H₁₉N₃O
• Molecular Weight: 269.346
• Hs Code.: 2925290090
• Mol file: 16136-32-6.mol

Synonyms:Guanidine,(2-benzhydryloxyethyl);N-(2-Benzhydryloxy-aethyl)-guanidin;(2-BENZHYDRYLOXYETHYL)GUANIDINE;

Chemical Property of 1-[2-(Diphenylmethoxy)ethyl]guanidine

Chemical Property:

• Vapor Pressure: 1.37E-07mmHg at 25°C
• Refractive Index: 1.6500 (estimate)
• Boiling Point: 429.7°Cat760mmHg
• PKA: 12.74±0.70(Predicted)
• Flash Point: 213.7°C
• PSA: 71.13000
• Density: 1.13g/cm³
• LogP: 3.46660

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[2-(Diphenylmethoxy)ethyl]guanidine

There total 2 articles about 1-[2-(Diphenylmethoxy)ethyl]guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-Diphenylmethanol (91-01-0) + 2-methylisothiourea sulphate (14527-26-5,867-44-7,147895-43-0) + chloroacetonitrile (107-14-2) → N-(2-Benzhydryloxy-aethyl)-guanidin (16136-32-6)

Guidance literature:

Multistep reaction; (i) K₂CO₃, MeCOEt, (ii) LiAlH₄, Et₂O, (iii) /BRN= 3572707/;

DOI:10.1021/jm00342a017

Reference yield:

2-{[(diphenyl)methyl]oxy}ethylamine (17349-94-9) + 2-ethylisothiourea hydrobromide (1071-37-0,133514-72-4) → N-(2-Benzhydryloxy-aethyl)-guanidin (16136-32-6)

Guidance literature:

In chloroform;

upstream raw materials:

1,1-Diphenylmethanol

2-methylisothiourea sulphate

chloroacetonitrile

2-{[(diphenyl)methyl]oxy}ethylamine

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