Benzothiazole, 6-(1-piperidinyl)- (9CI)

Base Information

• Chemical Name: Benzothiazole, 6-(1-piperidinyl)- (9CI)
• CAS No.: 663627-30-3
• Molecular Formula: C12H14N2S
• Molecular Weight: 218.31800
• Hs Code.: 2934200090
• Mol file: 663627-30-3.mol

Synonyms:6-(N-piperidyl)benzothiazole;OGBXIDWJHRBZJK-UHFFFAOYSA;Benzothiazole,6-(1-piperidinyl);6-(piperidin-1-yl)benzo[d]thiazole;

Chemical Property of Benzothiazole, 6-(1-piperidinyl)- (9CI)

Chemical Property:

• PSA: 44.37000
• LogP: 3.35160
• Storage Temp.: 2-8°C

Purity/Quality:

98% ^*data from raw suppliers

6-piperidin-1-yl-1,3-benzothiazole 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzothiazole, 6-(1-piperidinyl)- (9CI)

There total 2 articles about Benzothiazole, 6-(1-piperidinyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-aminophenyl)piperidine dihydrogen sulfate → 6-(piperidin-1-yl)benzo[d]thiazole (663627-30-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium thiosulfate pentahydrate; potaasium dichromate; acetic acid / H₂O

2: 305 mg / 3 h / Heating

With potassium dichromate; sodium thiosulfate; acetic acid; In water;

DOI:10.1016/j.tet.2003.11.020

Reference yield:

formic acid (64-18-6) + 2-amino-5-piperidin-1-yl-benzenethiol → 6-(piperidin-1-yl)benzo[d]thiazole (663627-30-3)

Guidance literature:

for 3h; Heating;

DOI:10.1016/j.tet.2003.11.020

Reference yield: 94.0%

bromobenzene (108-86-1,52753-63-6) + 6-(piperidin-1-yl)benzo[d]thiazole (663627-30-3) → C18H18N2S (1218788-78-3)

Guidance literature:

With dichlorobis(chlorodi-tert-butylphosphine) palladium(II); Cu[9,9-dimethyl-4,5-bis(diphenylphosphine)xanthene]I; caesium carbonate; In toluene; at 100 ℃; Inert atmosphere;

DOI:10.1021/ja100354j

upstream raw materials:

formic acid

Downstream raw materials:

C₁₈H₁₈N₂S

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