4-Phenyl-1H-iMidazol-2-aMine hydrochloride

Base Information

Chemical Name:4-Phenyl-1H-iMidazol-2-aMine hydrochloride
CAS No.:6653-43-6
Molecular Formula:C9H9N3.ClH
Molecular Weight:195.64900
Hs Code.:2933290090
Mol file:6653-43-6.mol

Synonyms:4-Phenyl-1H-imidazol-2-amine hydrochloride;2-amino-4-phenyl-1H-imidazole hydrochloride;

Suppliers and Price of 4-Phenyl-1H-iMidazol-2-aMine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-Phenyl-1H-imidazol-2-aminehydrochloride 95+%
1g
$ 581.00

Chemenu
4-phenyl-1H-imidazol-2-aminehydrochloride 95%
1g
$ 549.00

Alichem
4-Phenyl-1H-imidazol-2-aminehydrochloride
1g
$ 516.66

Total 6 raw suppliers

Chemical Property of 4-Phenyl-1H-iMidazol-2-aMine hydrochloride

Chemical Property:

PSA：55.43000
LogP:2.39100
Storage Temp.:Sealed in dry,Room Temperature

Purity/Quality:

95% ^*data from raw suppliers

4-Phenyl-1H-imidazol-2-aminehydrochloride 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Phenyl-1H-iMidazol-2-aMine hydrochloride

There total 4 articles about 4-Phenyl-1H-iMidazol-2-aMine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: tert-butyl 2-amino-4-phenyl-1H-imidazol-1-carboxylate

: 6653-43-6
2-amino-4-phenyl-1H-imidazole hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; ethyl acetate; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2010.05.074

Reference yield:

: 70-11-1
α-bromoacetophenone

: 219511-71-4
tert-butyl N-(diaminomethylidene)carbamate

: 6653-43-6
2-amino-4-phenyl-1H-imidazole hydrochloride

Guidance literature:: α-bromoacetophenone; tert-butyl N-(diaminomethylidene)carbamate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

With hydrogenchloride; In methanol;
DOI:10.1002/cmdc.201900033

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 6653-43-6
2-amino-4-phenyl-1H-imidazole hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.1: 1 h / 0 °C

2.2: 0.33 h / 0 °C

3.1: N,N-dimethyl-formamide / 48 h / 20 °C

3.2: 2 h / 20 °C

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201900033