Cyclohexanimine, N-chloro-

Base Information

• Chemical Name: Cyclohexanimine, N-chloro-
• CAS No.: 6681-70-5
• Molecular Formula: C6H10ClN
• Molecular Weight: 131.605
• Mol file: 6681-70-5.mol

Synonyms:

Chemical Property of Cyclohexanimine, N-chloro-

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanimine, N-chloro-

There total 11 articles about Cyclohexanimine, N-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

cyclohexylamine (108-91-8,157973-60-9) → cyclohexyl-N-chloroketimine (6681-70-5)

Guidance literature:

With TEA; trichloroisocyanuric acid; In N,N-dimethyl-formamide; at 15 ℃; for 4h;

DOI:10.1055/s-2004-830896

Reference yield: 77.0%

N-dichlorocyclohexylamine (26307-01-7) → cyclohexyl-N-chloroketimine (6681-70-5)

Guidance literature:

With TEA; In dichloromethane; at 25 ℃; for 2h;

DOI:10.1055/s-2004-830896

Reference yield: 48.0%

N-dichlorocyclohexylamine (26307-01-7) → cyclohexyl-N-chloroketimine (6681-70-5) + cyclohexene (110-83-8)

Guidance literature:

DOI:10.1021/jo00334a001

upstream raw materials:

N-dichlorocyclohexylamine

cyclohexanone

C₇H₁₂Cl₂N₂O

1-oxa-2-azaspiro[2.5]octane

Downstream raw materials:

3,3-pentamethylenediaziridine